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Gozzi, Christel; Bouzidi, Naoual – Journal of Chemical Education, 2008
The aim of this experiment is to study and calculate the kinetic constant of a Heck reaction: the arylation of but-3-en-2-ol by iodobenzene catalyzed by palladium acetate in presence of triethylamine in DMF. The reaction leads to a mixture of two ketones. Students use GC analysis to quantify reagents and products of reaction. They control the…
Descriptors: Kinetics, Organic Chemistry, Laboratory Experiments, Molecular Structure