High-performance liquid chromatography (HPLC) experiments are an important part of the undergraduate analytical instrumentation laboratory courses and usually use commercial C18 silica-packed reversed-phase columns. In this experiment, a simple method of preparing SiO[subscript 2] core-shell packed columns was developed to enable students to…

We present a simple undergraduate level experiment dealing with the preparation and characterization of a colloidal Langmuir-Blodgett (LB) film. The experiment is designed to invoke an interdisciplinary understanding of colloid chemistry and surface science. It will allow the students to develop the concepts of wettability, hydrophobicity, and…

Metal-organic frameworks (MOFs) are a class of porous materials that are often crystalline with high surface area and structural tunability. In this laboratory experiment designed for inorganic chemistry students at the undergraduate level, students complete a two-step experiment where they will first (i) synthesize two isostructural…

A comprehensive teaching experiment plan tailored forthird-yearundergraduates has been developed. Initially, instructors synthesize(E)-2-(4-((4-(2-hydroxyethoxy)-3-methylphenyl)­diazenyl)­phenoxy)-ethan-1-ol­(M-Azo-2)monomer as part of the preclass preparation. Subsequently, studentsperform an acylation reaction experiment to prepare an…

The substitution of carbonyl compounds with liquid bromine as a brominating agent is the most commonly employed synthesis method for a-bromoacetophenone and its derivatives. However, liquid bromine possesses certain drawbacks, such as volatilization, high toxicity, strong corrosion, and poor reaction selectivity, which limit its application and…

In analytical chemistry, discussing different method sand techniques of analysis is essential to promote critical thinking and reasoning. Analytical courses in the chemist, pharmacist, and biochemist curricula represent the opportunity to study concepts such as experimental design, sampling, development, and optimization of protocols, data…

In view of the mounting requirements for courses in nuclear chemistry and radiochemistry, hands-on experience in the separations of radioisotopes is imperative. Three separation techniques commonly used were introduced, coprecipitation, liquid-liquid extraction, and ion-exchange chromatography. Their principles and the associated fundamental…

In chemistry, a eutectic mixture refers to a mixture of two or more components at which the lowest possible freezing point is observed. This phenomenon is covered in a wide range of curricula such as physics, chemistry, chemical engineering, and pharmacy to various depths. Despite the significance of this phenomenon in pharmaceutical compounding…

Calculating analytical uncertainties as a part of method validation is a relevant aspect of field and laboratory practices in instrumental analytical chemistry subjects, which usually require complex algorithms. This work describes the development and didactic use of an automatic and straightforward informatics tool, implemented in an Excel macro,…

This paper addresses the fundamentals, structuring, and application of a Formative Dimensions for Green and Sustainable Chemical Education (Formative Dimensions -- GSCE) qualitative evaluation tool of experimental processes. This instrument was created considering the need to resignify laboratory practices in Chemical Education. Qualitative…

Titration is an important experimental skill that every chemistry educator and learner must master. Titration is often the method of choice in the science laboratory courses in secondary and postsecondary schools. During acid-base titration, chemistry learners are always told about salt formation. However, a practical visualization of the salt…

The classic silver mirror reaction at room temperature in textbooks usually used glucose to react with silver nitrate and ammonium nitrate with the presence of caustic alkalis. But the aldehydes such as acetaldehyde and propionaldehyde were difficult to react under the same condition. In this paper, Na[subscript 2]CO[subscript 3] was used to…

This article seeks to provide researchers and practitioners in laboratory education, particularly those involved in the curriculum design and implementation of teaching laboratories at university level, with a conceptual framework and a working model for an integrated assessment of learning domains, by attending to a more holistic approach to…

We present a novel method for demonstrating the physical principles of ultrasound imaging at a level suitable for educational programmes up to the university level, using a simple mechanical model that is very inexpensive and accessible to a broad variety of educational institutions. The method revolves around the use of one or two steel springs…

Physics preparation for primary school teachers has received attention only in recent decades. Research on science education provides useful guidelines, often disregarded. Several interrelated research questions must be addressed by field research, namely, (a) which physics subjects to teach in primary school and its relationships with other…