In this guided inquiry experiment, students extract catecholase enzyme from apples to catalyze the oxidation of catechol. They follow the reaction using the UV--vis absorbance of the "p"-benzophenone produced to determine the Michaelis-Menten kinetic parameters. Students make selected experimental choices within a structured framework…

At first glance, scientific laboratory experiences might appear to be challenging to move to the cloud. Skeptics may point to sensory feedback limitations and inequivalence of student outcomes. However, emerging data increasingly provide evidence that scientific laboratory courses are not only amenable to online learning, but also can deliver…

A revised version of a traditional physical chemistry laboratory experiment has been developed to enhance student discussion in the laboratory and to improve students' connections between physical chemistry concepts and real molecular systems. In this experiment, students explore the keto-enol tautomerization of 2,4-pentanedione. However, unlike…

More than ever, there is an increasing need for digital experimental learning environments in chemistry. The variety of digital learning approaches provided to students range from simple videos showing experiments to highly interactive virtual laboratories. Regardless of which approach is chosen, a digital learning environment should be adapted to…

Laboratory safety is a vital part of a chemical education and can be incorporated into courses throughout the chemistry curriculum. Discussions of laboratory safety can serve as an introduction to the important field of green chemistry. Exposure to this field can better prepare students for safer and more sustainable laboratory practices in…

Remote delivery approaches to laboratory courses in the response to the COVID-19 pandemic have included a spectrum spanning passive options such as providing students with prerecorded videos of experiments to replacing in-person laboratory experiences with immersive virtual reality environments. While interactive activities that require students…

We present an experiment designed to hone the decision-making skills of (undergraduate) chemistry students by using aqueous crossed aldol reactions. Here, we present two simple crossed aldol reactions based on inexpensive and readily available materials: The condensation of vanillin and cinnamaldehyde with acetone. The procedure uses the variation…

Selecting less hazardous chemicals is a core tenet of green chemistry but is difficult to teach in practice. The upper-year undergraduate or graduate level exercise described here empowers students to make such decisions themselves. Students are tasked with finding the greenest chemical for a specific purpose described in a hypothetical scenario,…

[superscript 31]P{[superscript 1]H} nuclear magnetic resonance spectroscopy is a particularly useful tool for studying the reactions of P-donor ligands such as phosphines and phosphites with transition metals and other Lewis bases because the reactions take place on the nonbonding pair of electrons on the phosphorus. In addition, [superscript 31]P…

A lab activity for teaching physics students the fundamentals of statistical analysis during the first few weeks of instruction is described. This activity involves students timing a pulse of light generated by an Arduino device of fixed duration with individual timers (e.g. stopwatch, iPhone timer). To select the most precise timing methods and…

Because traditional laboratory practices in advanced chemistry education are being replaced by inquiry-based approaches, we present herein a new laboratory activity based on a small research project that was designed and executed by students. The laboratory project aims at answering a well-defined research question: how far can potentiometric…

The method of least squares (LS) yields exact solutions for the adjustable parameters when the number of data values n equals the number of parameters "p". This holds also when the fit model consists of "m" different equations and "m = p", which means that LS algorithms can be used to obtain solutions to systems of…

A guided-inquiry experiment was designed and implemented in an introductory organic chemistry laboratory course. Students were given a mixture of compounds and had to isolate two of the components by designing a viable workup procedure using liquid-liquid separation methods. Students were given the opportunity to apply their knowledge of chemical…

Although much of the scientific community concerns itself with ideas of a sustainable future, very little of this interest and motivation has reached the classroom experience of the average chemistry major, and therefore, it is imperative to expose students to these ideas early in their careers. The focus of most undergraduate chemistry curricula…

Chemical engineering is rarely encountered before higher-level education in the U.S. or in Europe, leaving prospective students unaware of what an applied chemistry or chemical engineering degree entails. In this lab experiment, we report the implementation of a three-day course to showcase chemical engineering principles for 16-17 year olds…