A major challenge when designing new experiments for the general chemistry laboratory is introducing students to the necessary techniques while keeping the experiment engaging and accessible. This work presents a new multiweek activity designed to introduce students to advanced instrumentation in the form of high-performance liquid chromatography…

A chemistry laboratory experiment is described to introduce undergraduate college students to membrane separation technology. This experiment combines a simple nanowire membrane fabrication and visually indicated molecule separation. The membrane is produced via coprecipitation synthesis followed by a filtration assembly process, which can be…

Photochemical reactions are the reactions that are induced by light. Many of these reactions are found in natural processes, including photosynthesis and the formation and decomposition of ozone in the atmosphere. Classroom demonstrations are effective in enhancing students' learning and retention. Herein, we have developed a simple demonstration…

Lakes are artists' pigments made from colorants bound to an inert substrate, usually hydrated aluminum oxide. Before the late 19th century, lakes were made from natural pigments extracted from plants and insects, extracted either directly from the dyestuff or indirectly from waste materials generated in the manufacture of dyed textiles. The first…

This experiment demonstrates that copper(II) chloride dihydrate (CuCl[subscript 2]·2H[subscript 2]O) in different solvents (acetone, isopropyl alcohol, or water) displays divergent colors and visible-near IR spectra. Both the reactions of these solutions with 2 equiv of sodium hydroxide (NaOH) and the direct solid-state reaction of CuCl[subscript…

There is an increasing need for fundamental electrochemistry concepts to be taught in the undergraduate curriculum, given the broad applicability of electrochemical technologies in addressing a wide range of global issues from critical energy shortages to real-time medical diagnostics. However, many electrochemical concepts are often taught in…

Electrochromism encompasses reversible changes of material's optical properties (color, opacity) under the influence of an external electric current or applied voltage. The effect has been known for decades, but its importance continues to grow due to the rapid development of smart systems and the accompanying demand to build devices that consume…

So-called "Color Wonder" markers contain colorless dyes that only display color when used to mark on special "Color Wonder" paper. These markers make use of leuco dyes that only develop color in the presence of acid. These markers provide science educators with a novel chemical system that can be implemented in inquiry-based…

This is an easy and inexpensive laboratory experiment in which undergraduate students at the Bachelor's degree level in Chemistry can measure formation constants of complexes [Ni(en)[subscript n](OH[subscript 2])[subscript 6-2n]][superscript 2]+ (n = 1, 2 or 3; en = ethylenediamine) through an acid-base titration. The background information…

Herein, we describe a simple laboratory experiment to address nanomaterial synthesis, plasmon resonance, and its application to detect Cu[superscript 2+] in ultralow concentrations. The proposed experiment is very visual and appealing for chemistry students, especially the undergraduate-level chemistry major. In this experiment, the aggregation of…

The laboratory experiment presented here describes the use of a calcium ion-selective electrode (Ca-ISE) to determine the concentration of zinc in a supplement tablet. This approach was developed to show students how to expand the range of applications of Ca-ISE to enable the determination of metal ions other than Ca[superscript 2+]. To determine…

There has been dramatic growth in interest and research regarding organic photochromism in recent decades. Despite this, the topic is seldom addressed in the undergraduate chemistry curriculum. Herein, we present a straightforward and robust experiment for the second semester organic chemistry laboratory curriculum which combines multistep…

A fast, operationally simple, and reproducible synthetic protocol for anthraquinone dyes (AQDs), suitable for upper-division undergraduate industrial and organic chemistry laboratory courses, has been developed. This experiment is composed of three stages; the first step deals with the synthesis of AQDs, followed by a purification step, and…

In light of the COVID-19 pandemic situation, the separation of the primary colors of ink markers and food coloring was performed using a simplified column chromatography setup at home to accomplish the educational outcome of the course. The virtual class instruction, for the students enrolled in the "Organic Techniques Laboratory"…

Colorful transitions of various acid-base indicators have been used to illustrate the concept of chemical equilibria, especially in spectrophotometric determination of the equilibrium constants or pKa values. To accommodate an online laboratory environment necessitated by the COVID-19 pandemic, this work employs color analyses from digital images…