A public demonstration of laser ablation inductively coupled plasma mass spectrometry (LA-ICPMS) for fast and sensitive qualitative elemental analysis of solid everyday objects is described. This demonstration served as a showcase model for modern instrumentation (and for elemental analysis, in particular) to the public. Several steps were made to…

An instrumentation-based laboratory curriculum combining traditional unknown analyses with student-designed projects has been developed for an introductory analytical chemistry course. In the first half of the course, students develop laboratory skills and instrumental proficiency by rotating through six different instruments performing…

The teaching of instrumental analysis for many small colleges and high schools continues to be stymied by high-cost, complicated maintenance, high power requirements, and often the sheer bulk of the instrumentation. Such issues have led us to develop inexpensive instruments as part of a SMILE initiative (small, mobile instruments for laboratory…

We present a simple, effective, and inexpensive spectrophotometer design that may be used in a stand-alone teaching module, and to enhance various unit operations experiments. The spectrophotometers described performed as well as a commercial option at estimating cell concentration in a bioreactor and tracking a first-order reaction. Such devices…

A new lecture/laboratory course to offer advanced biochemical training for undergraduate and early graduate students has been developed in the Department of Chemistry at the University of Nebraska at Omaha. This unique course offers students an opportunity to work hands-on with modern instrumentation not normally found in a predominately…

Note is presented on the standard lab from a second year chemistry course. The lab "Determining which of the Seven FD&C Food-Approved Dyes are Used in Making Green Skittles", familiarizes students with the operation of the CHEM2000 UV-Vis spectrophorometer.

Using fourier transformation methods in nuclear magnetic resonance has made possible increased sensitivity in chemical analysis. This article describes these methods as they relate to magnetization, the RF magnetic field, nuclear relaxation, the RF pulse, and free induction decay. (CW)

Discussed are two techniques that can be used to directly test the theory that the plates which make up the crust of the earth are still moving. Described are the use of satellite laser ranging and very long baseline interferometry. Samples of data and their analysis are provided. (CW)

Using Fourier transformation methods in nuclear resonance has made possible increased sensitivity in chemical analysis. This article describes data acquisition, data processing, and the frequency spectrum as they relate to this technique. (CW)

Microcomputers are commonly interfaced to external devices in scientific, industrial, and consumer settings for data acquisition and for control. The general problem under consideration is the task of taking measurements of some continuous phenomenon, transforming them into digital form, and storing the data in the microcomputer for later use.…

Describes an experimental procedure to measure the specific heat of a gas. Discusses equipment, setup, and procedures and provides sample values obtained for air, propane, helium, carbon dioxide, and argon. (JM)

A laboratory experiment designed as a model for studying enzyme activity with a basic spectrometer is presented. Included are background information, experimental procedures, and a discussion of probable results. Stressed is the value of the use of Nuclear Magnetic Resonance in biochemistry. (CW)

Described is a case, a heterocyclic sulfoxide, which is useful for an introduction to first-order four-spin data analysis. Background of this technique for use with undergraduate students is given including a sample analysis, a list of supplementary materials, and experimental procedures. (CW)

Describes a simple method for determining self-inductance of non-ferromagnetic rings. Suggests fitting the ring with an auxiliary coil and using a solenoid driven with a known frequency alternating current. Amplitude change and phase shift can be measured and used to calculate inductance. Material list, calculations, and sample results are given.…

Presents a method of constructing short range transmitters suitable for sensing the temperature in eggs, nest cavities or other applications. Provides a list of materials, circuit diagram, and assembly instructions. (CW)