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ERIC Number: EJ1445661
Record Type: Journal
Publication Date: 2023-Sep
Pages: 7
Abstractor: As Provided
ISBN: N/A
ISSN: ISSN-0021-9584
EISSN: EISSN-1938-1328
Available Date: N/A
A Raspberry Pi Pico Based Low-Cost, Research-Grade, Open-Source Thermal Conductivity Cell Detector for Chemical Laboratory Analysis
Yuxin Chen; Yuting Wu; Zhengwen Li; Yanyan Zheng; Binhang Yan; Yi Cheng
Journal of Chemical Education, v100 n9 p3477-3483 2023
The "maker" movement is gaining widespread attention, especially in the field of laboratory education. Here we have built a low-cost, "do-it-yourself", open-source thermal conductivity cell detector (TCD) for chemical laboratory analysis, which is assembled from thermal conductivity gas sensor elements and 3D-printed flow cell parts based on a Raspberry Pi Pico microcontroller. An ADS1115 digital-to-analog converter (with 16-bit acquisition resolution) is used to acquire the electrical signal from the thermal conductivity sensor response via a Wheatstone bridge. The device is programmed to acquire data based on the open-source Thonny Micro Python IDE software via I[superscript 2]C communication. Temperature programming analysis (TPA) is an important technique to characterize heterogeneous catalysts; therefore, we apply the assembled TCD to characterize the reduction properties of commercial Cu/ZnO/Al[subscript 2]O[subscript 3] catalysts. The hydrogen temperature-programmed reduction (H[subscript 2]-TPR) profile of the commercial Cu/ZnO/Al[subscript 2]O[subscript 3] catalyst shows a broad peak in the range of 150--250 °C with a peak position at 213 °C, which is consistent with previous reports. The total amount of hydrogen consumed by the commercial catalyst during H[subscript 2]-TPR is 10.7 mmol/g[subscript cat], which can be calculated from the calibrated H[subscript 2] vol % TCD signal result and the peak area of the H[subscript 2]-TPR profile. The results show that the fabricated TCD detector exhibits excellent performance during the testing process and is capable of meeting research-grade applications. In summary, students will learn a wide range of skills in a hands-on learning environment of a chemistry laboratory course.
Division of Chemical Education, Inc. and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
Publication Type: Journal Articles; Reports - Descriptive
Education Level: N/A
Audience: N/A
Language: English
Sponsor: N/A
Authoring Institution: N/A
Grant or Contract Numbers: N/A
Author Affiliations: N/A