ERIC Number: EJ1445661
Record Type: Journal
Publication Date: 2023-Sep
Pages: 7
Abstractor: As Provided
ISBN: N/A
ISSN: ISSN-0021-9584
EISSN: EISSN-1938-1328
Available Date: N/A
A Raspberry Pi Pico Based Low-Cost, Research-Grade, Open-Source Thermal Conductivity Cell Detector for Chemical Laboratory Analysis
Yuxin Chen; Yuting Wu; Zhengwen Li; Yanyan Zheng; Binhang Yan; Yi Cheng
Journal of Chemical Education, v100 n9 p3477-3483 2023
The "maker" movement is gaining widespread attention, especially in the field of laboratory education. Here we have built a low-cost, "do-it-yourself", open-source thermal conductivity cell detector (TCD) for chemical laboratory analysis, which is assembled from thermal conductivity gas sensor elements and 3D-printed flow cell parts based on a Raspberry Pi Pico microcontroller. An ADS1115 digital-to-analog converter (with 16-bit acquisition resolution) is used to acquire the electrical signal from the thermal conductivity sensor response via a Wheatstone bridge. The device is programmed to acquire data based on the open-source Thonny Micro Python IDE software via I[superscript 2]C communication. Temperature programming analysis (TPA) is an important technique to characterize heterogeneous catalysts; therefore, we apply the assembled TCD to characterize the reduction properties of commercial Cu/ZnO/Al[subscript 2]O[subscript 3] catalysts. The hydrogen temperature-programmed reduction (H[subscript 2]-TPR) profile of the commercial Cu/ZnO/Al[subscript 2]O[subscript 3] catalyst shows a broad peak in the range of 150--250 °C with a peak position at 213 °C, which is consistent with previous reports. The total amount of hydrogen consumed by the commercial catalyst during H[subscript 2]-TPR is 10.7 mmol/g[subscript cat], which can be calculated from the calibrated H[subscript 2] vol % TCD signal result and the peak area of the H[subscript 2]-TPR profile. The results show that the fabricated TCD detector exhibits excellent performance during the testing process and is capable of meeting research-grade applications. In summary, students will learn a wide range of skills in a hands-on learning environment of a chemistry laboratory course.
Descriptors: Costs, Open Educational Resources, Chemistry, Science Laboratories, Shared Resources and Services, Printing, Information Technology, Programming, Scientific Concepts, Science Education, Scientific Research, Hands on Science, Laboratory Experiments
Division of Chemical Education, Inc. and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
Publication Type: Journal Articles; Reports - Descriptive
Education Level: N/A
Audience: N/A
Language: English
Sponsor: N/A
Authoring Institution: N/A
Grant or Contract Numbers: N/A
Author Affiliations: N/A