General chemistry courses serve as foundational curriculum within most STEM undergraduate curricula, and hence, it is essential to assess student knowledge and application of learning outcomes for courses such as Introduction to Chemistry and Organic Chemistry. Within the United States, paper-and-pencil examinations are typical for measuring…

In this paper, the development of an automatic assessor is presented, both in MATLAB and in Excel, for an analytical exercise. In particular, the emulation of an interlaboratory exercise, using the analytical determination of phosphorus in a dry detergent, carried out in the laboratory by different groups of students, was selected as a case of…

Most measurement techniques have some limitations imposed by a sensor's signal-to-noise ratio (SNR). Thus, in analytical chemistry, methods for enhancing the SNR are of crucial importance and can be ensured experimentally or established via pre-treatment of digitized data. In many analytical curricula, instrumental techniques are given preference…

A quantitative and qualitative study of the interplay between absorption, fluorescence, and excitation spectra of pollutants called polycyclic aromatic hydrocarbons (PAHs) is conducted. The study of five PAH displays the correlation of the above-mentioned properties along with the associated molecular changes.

Microscale fusions, description, and spectroscopic analysis of the reactivity of a square planar Cu(III) complex significant to green chemistry, are presented. The experiment also includes nine focal points on which pre-lab and post-lab questions are based, and the final exams reflect the students' comprehension of these and other features of…

Several data-analysis problems could be addressed in different ways, ranging from a series of related "local" fitting problems to a single comprehensive "global analysis". The approach has become a powerful one for fitting data to moderately complex models by using library functions and the methods are illustrated for the analysis of HCI-IR…

Qualitative analysis schemes are used in undergraduate laboratory settings as a way to introduce equilibrium concepts and logical thinking. The main component of all qualitative analysis schemes is a flame test, as the color of light emitted from certain elements is distinctive and a flame photometer or spectrophotometer in each laboratory is…

Reviews background of atomic absorption spectrometry techniques. Discusses problems encountered and precautions to be taken in determining trace elements in the parts-per-billion concentration range and below. Concentrates on determining chromium in biological samples by graphite furnace atomic absorption. Considers other elements, matrices, and…