Virtually all modern chemical instrumentation is controlled by computers. While software packages are continually becoming easier to use, allowing for more researchers to utilize more complex instruments, conveying some level of understanding as to how computers and instruments communicate is still an important part of the undergraduate…

For most chemistry curricula, laboratory-based activities in quantitative and instrumental analysis continue to be an important aspect of student development/training, one that can be more effective if conceptual understanding is delivered through an inquiry-based process relating the material to relevant issues of public interest and student…

The teaching of instrumental analysis for many small colleges and high schools continues to be stymied by high-cost, complicated maintenance, high power requirements, and often the sheer bulk of the instrumentation. Such issues have led us to develop inexpensive instruments as part of a SMILE initiative (small, mobile instruments for laboratory…

Access to state-of-the-art instrumentation, namely nuclear magnetic resonance (NMR) spectroscopy, early in the college curriculum was provided to undergraduate students in an effort to improve student perceptions of science. Proton NMR spectroscopy was introduced as part of an aspirin synthesis in a guided-inquiry approach to spectral…

Students' attitudes toward and conceptual understanding of chemical instrumentation is surveyed. The study shows that, in general, the students' attitudes toward using instrumentation in the lab is quite positive and they felt that using instrumentation in the lab allowed them not only to connect "chemistry" and the "real world", but also to…

A variety of methods for producing images and some of the tools available for image analysis are described. (BB)

One undergraduate chemistry laboratory at the California Institute of Technology is described, including goals of the laboratory curriculum: (1) emphasis on modern instrumental methods of analysis, separation, and characterization; (2) integration of organic/inorganic experiments; and (3) preparing students in two years to begin work in a research…

A kit is described for use in automation of routine chemical research procedures. The kit uses sensors to evaluate the state of the system, actuators which modify the adjustable parameters, and an organ of decision which uses the information from the sensors. (BB)

Greater access to scientific instrumentation, courses, and supporting materials through the Internet and Integrated Laboratory Network (ILN) has the potential to profoundly change the way in which instrumental sciences are taught. Increased access to instrumentation will provide better opportunities for students to learn and practice instrumental…

Describes an experiment combining qualitative and quantitative information from hydrogen nuclear magnetic resonance spectra. Reviews theory, discusses the experimental approach, and provides sample results. (JM)

Discusses the value of electrophoresis in the fields of protein chemistry and biochemistry. Describes how to build an inexpensive electrophoresis setup for use in either research or teaching activities. Details the construction of both the separating device and the power supply. (TW)

This report presents priorities for new facilities and new capabilities at existing facilities with initial costs of at least $5 million. The new facilities in order of priority are: (1) a 6 GeV synchrotron radiation facility; (2) an advanced steady state neutron facility; (3) a 1 to 2 GeV synchrotron radiation facility; and (4) a high intensity…

Describes the construction of a low-cost (about $70.00) alternative to the commercial fraction collector. Outlines the separate parts of the collector and provides a schematic of electronic circuitry of the instrument. Lists special items required for the development of this project. (TW)