Herein we describe an accessible and safe at-home experiment to separate lycopene from tomatoes via liquid-liquid extraction. As a qualitative experiment, it is a canonically elementary instance for high school students to digest the conception of miscibility, immiscibility, and density difference of the two solvents. This experiment was performed…

The variation in the transference number of H[superscript +] (aq) is investigated for different HCl solution concentrations. The method for scribing graduations on electromigration tubes is modified to decrease the error in experimental measurements, and metallic copper is used as the anode to reduce the toxicity and environmental impact of the…

Photochemical reactions are initiated by the absorption of light, triggering the chemical reactions and resulting in the formation of products. These reactions are generally performed using a freely available renewable source of energy-solar energy. Solar simulators mimic both the ultraviolet and visible regions of sunlight and hence can serve as…

The substitution of carbonyl compounds with liquid bromine as a brominating agent is the most commonly employed synthesis method for a-bromoacetophenone and its derivatives. However, liquid bromine possesses certain drawbacks, such as volatilization, high toxicity, strong corrosion, and poor reaction selectivity, which limit its application and…

We have developed a guided-inquiry laboratory exercise in which students perform viscosity measurements to infer the structure of poly(vinyl alcohol) (PVA) in aqueous solution. The activity combines both experiments and modeling. In the experimental portion of the exercise, students measure the viscosity of several solutions of PVA with differing…

Starting with a double replacement reaction in alcohol between Ni(H[subscript 2]O)[subscript 6](NO[subscript 3])[subscript 2] and NaX, students exploit solubility differences to produce a solution of NiX[subscript 2] and a NaNO[subscript 3] precipitate. They then synthesize a bis(N,N-diethylethylenediamine) Ni(II) complex with chloride, bromide,…

Removing the pollutants from various wastewater is crucial to the environment, ecology, and humans. However, the pollutants are generally removed by chemical decomposition, which not only consumes a lot of energy but also produces carbon emissions. Electrochemical flocculation is effective to extract pollutant molecules and heavy ions from…

In analytical chemistry, discussing different method sand techniques of analysis is essential to promote critical thinking and reasoning. Analytical courses in the chemist, pharmacist, and biochemist curricula represent the opportunity to study concepts such as experimental design, sampling, development, and optimization of protocols, data…

A procedure to purify anthocyanin, a natural pigment, following a green approach by using macroporous resin and its encapsulation for the maintenance of its stability is described. This laboratory experiment, which describes the benefits of using resin for the purification, is a learning tool for students working in the field on nutraceuticals.…

Calculating analytical uncertainties as a part of method validation is a relevant aspect of field and laboratory practices in instrumental analytical chemistry subjects, which usually require complex algorithms. This work describes the development and didactic use of an automatic and straightforward informatics tool, implemented in an Excel macro,…

The chemical experiment in this study is specifically created for undergraduate students studying energy and the environment. The target of the experiment is for students to comprehend the deactivation mechanism of the Ce/TiO[subscript 2] catalyst by oxides of phosphorus through practical experiments and enhance their knowledge of environmental…

This manuscript describes a laboratory exercise that allows students to use conductive atomic force microscopy (CAFM) for the analysis of electrodeposited, metallic structures. In addition to nanoscale electrical characterization with CAFM, this laboratory exercise also provides students with an opportunity to explore nanofabrication by…

The flue gas from waste incineration power plants contains high-level zinc species that may deactivate the catalyst for selective catalytic reduction (SCR) of nitrogen oxides (NO[subscript x]) with NH[subscript 3]. A comparison experiment was designed to investigate the effect of different types and Zn/Ce molar ratios on the performance of…

A laboratory experiment was designed to introduce the practical application of biocatalysis in Bachelor and Master courses in biotechnology and medicinal chemistry, respectively. To this aim, the lipase from "Candida rugosa" was characterized (protein concentration and activity), immobilized on a carrier (by hydrophobic adsorption), and…

This paper outlines a comprehensive teaching laboratory course program that centers on titration analysis, a timeless and essential technique in analytical chemistry spanning various disciplines, such as environmental science, medicine, and industry. In these fields, titration analysis is paramount for determining the concentrations of substances…