Students in a typical instrumental analysis course may learn more than 30 analytical techniques. There are more than 150 components associated with the instrumentation that they learn. To help students organize this large amount of information, we classified these components into four categories: sources, samples, discriminators, and detectors. In…

Gas chromatography-mass spectrometry (GC-MS) is a powerful analytical tool for detection, identification, and quantification of many volatile organic compounds. However, many colleges and universities have not fully incorporated this technique into undergraduate teaching laboratories despite its wide application and ease of use in organic…

Voltammetry is used as a model for teaching chemical instrumentation to chemistry undergraduates at the National University of Singapore. Lists six criteria used to select a successful teaching model and shows how voltammetry satisfies each criterion. (JN)

Describes a procedure for teaching undergraduate instrumental analysis laboratories to help minimize student confusion about the instruments. Handouts are distributed prior to the experiments and a thorough discussion of the instruments is given at the beginning of the experiment, followed by a demonstration of the instrument by the instructor.…

Discussed are two techniques that can be used to directly test the theory that the plates which make up the crust of the earth are still moving. Described are the use of satellite laser ranging and very long baseline interferometry. Samples of data and their analysis are provided. (CW)

Discussed is some of the confusion encountered in electrochemistry due to misunderstandings of sign conventions and simple mathematical errors. Clarified are issues involving emf series, IUPAC sign conventions, calculation of cell potentials, reference electrodes, the polarity of electrodes in electrochemical devices, and overpotential. (CW)

Explains some experiments involving thermal methods of analysis for undergraduate chemistry laboratories. Some experiments are: (1) the determination of the density and degree of crystallinity of a polymer; and (2) the determination of the specific heat of a nonvolatile compound. (HM)

Instructional videocassettes can provide efficient learning about analytical instrument maintenance and usage for scientists and technicians. Advantages of this approach include low cost to consumers, step-by-step instructions, and quality control of training. The programs currently available from three companies selling gas chromatographs and…

Discussed are selected application and future trends in supercritical fluid chromatography (SFC). The greatest application for SFC involves those analytes that are difficult to separate using GC or LC methods. Optimum conditions for SFC are examined. Provided are several example chromatograms. (MVL)

Presented is a simple laboratory set-up for teaching microprocessor-controlled data acquisition as a part of an instrumental analysis course. Discussed are the experimental set-up, experimental procedures, and technical considerations for this technique. (CW)

Presents a low cost system with easily replaced electrodes for use in general chemistry. Notes the accuracy and wide applicability permit easy use in physical or quantitative chemistry experiments. Provides schematic, theory, and helpful suggestions. (MVL)

Presents a model system designed for the electrophysiological investigation of single unit activity in intact anaesthetized animals. Illustrates how information is coded into action potential patterns by sense organs. Uses the ampullary electroreceptor of the brown bullhead catfish as an example. (Author/CW)

Elements covered in this review include: aluminum, antimony, arsenic, bismuth, boron, calcium, carbon, chromium, cobalt, copper, hydrogen, iron, lead, magnesium, manganese, molybdenum, nickel, niobium, nitrogen, oxygen, phosphorus, platinum, rare earths, silicons, sulfur, tin, titanium, tungsten, vanadium, zinc, and zirconium. Analytical methods…

Describes a graduate engineering course which specializes in model predictive control. Lists course outline and scope. Discusses some specific topics and teaching methods. Suggests final projects for the students. (MVL)

Announces the incorporation of a laboratory information management system (LIMS) into the academic environment. Describes the applications of a computer-automated laboratory system at one university. Stresses the benefits to students of the use of such a system in terms of entry into the industrial environment and to professors in grading. (CW)