A comprehensive teaching experiment plan tailored forthird-yearundergraduates has been developed. Initially, instructors synthesize(E)-2-(4-((4-(2-hydroxyethoxy)-3-methylphenyl)­diazenyl)­phenoxy)-ethan-1-ol­(M-Azo-2)monomer as part of the preclass preparation. Subsequently, studentsperform an acylation reaction experiment to prepare an…

The substitution of carbonyl compounds with liquid bromine as a brominating agent is the most commonly employed synthesis method for a-bromoacetophenone and its derivatives. However, liquid bromine possesses certain drawbacks, such as volatilization, high toxicity, strong corrosion, and poor reaction selectivity, which limit its application and…

This study's general theme revolves around practical work in chemical education, and its scope is the employment of a novel inquiry strategy combined with a new openness level. We investigate how the controlled positive error, a new device for inquiry activities developed by us, affects undergraduate students' experience of an experiment and…

A set of inexpensive and pedagogically rich experiments focusing on S[subscript N]1, E1, and E2 reactions have been updated to include modern computational and spectroscopic analyses. The S[subscript N]1 experiment involves treatment of "tert"-amyl alcohol with hydrochloric acid to generate the corresponding alkyl chloride, which is used…

Organic electrosynthesis is an increasingly popular tool for driving and probing redox reactions. Recent advances in this field often employ an electrocatalyst to enhance the selectivity and efficiency of electrochemical reactions. A laboratory experiment was developed to introduce students to relevant mechanistic techniques in electrochemistry…

In this article we consider the well-known demonstration of friction by two interleaved books. We consider a factor that has not been part of the popular explanation--atmospheric pressure. We provide three control experiments to demonstrate the role of atmospheric pressure in the two-book experiment and an additional simple demonstration of the…

Undergraduate laboratory courses, owing to their larger sizes and shorter time slots, are often conducted in highly structured modes. However, this approach is known to interfere with students' engagement in the experiments. To enhance students' engagement, we propose an alternative mode of running laboratory courses by creating some…

Graduate teaching assistants (GTAs) often lead laboratory and tutorial sections in science, technology, engineering, and mathematics (STEM), especially at large, research-intensive universities. GTAs' performance as instructors can impact student learning experience as well as learning outcomes. In this study, we observed 11 chemistry GTAs and 11…

A classic undergraduate introductory experiment is to measure the diffraction and interference pattern from single and double slits to determine slit width and separation. Studies show that Course-based Undergraduate Research Experiences (CUREs) can make science more inclusive when offered at the undergraduate level. Additionally, CUREs help…

Instructional labs are being transformed to better reflect authentic scientific practice, often by removing aspects of pedagogical structure to support student agency and decision making. We explored how these changes impact men's and women's participation in group work associated with labs through clustering methods on the quantified behavior of…

In the spring semester of 2020, colleges and universities adopted online teaching as the primary modality due to campus closure for social distancing. While lectures could be more readily converted to online classes, biology labs were challenging to handle since students could not physically conduct experiments in lab classrooms. In the present…

Students have been taught that atmospheric temperature drops linearly with altitude, up to approximately 15 km. However, even after completing an undergraduate degree program, most students have only memorized such information and have never had the experience of measuring it. Students often assume that experimental tasks must involve the use of…

Earth's field nuclear magnetic resonance (EFNMR) spectroscopy offers students a unique opportunity to consolidate their understanding of NMR spectroscopic theory through hands-on practice with a simple spectrometer. A comprehensive, 6 h experiment is presented for the introduction of low-field NMR techniques, covering spectroscopy, relaxivity, and…

Teaching emulsion polymerization is an important benchmark in undergraduate polymer courses. However, the introduction of hands-on experiments in undergraduate polymer laboratories is challenging: experimental time, reagents, and equipment involved are the primary restraints. We report a practical emulsion polymerization laboratory experiment for…

The stated purpose of this paper is to provide a simple and quick method to assemble pH electrodes using readily available materials. The present assembled electrodes are comparable with commercial pH electrodes, with accuracy for pH determination in the range 2-12. Furthermore, the constructed simple pH electrodes exhibit a fast and stable…