We present an experiment designed to hone the decision-making skills of (undergraduate) chemistry students by using aqueous crossed aldol reactions. Here, we present two simple crossed aldol reactions based on inexpensive and readily available materials: The condensation of vanillin and cinnamaldehyde with acetone. The procedure uses the variation…

A Unit Operations Laboratory (UOL) is fundamental to undergraduate chemical engineering education. This article discusses a new course structure for the University of Kansas UOL and details for three new experiments covering the fundamentals of vapor-liquid equilibrium, fluid mechanics, and kinetics. Students apply knowledge from these courses as…

Describes a comparison of scale of laboratory with respect to time efficiency. Compared full scale and one-tenth scale Grignard reactions with full scale averaging 330 minutes to completion and scaled-down averaging 204. Savings are seen in air pollution, toxicity, solvent cost, and time. (JM)