An active-learning approach was employed in a project for our chemistry major students on the synthesis of biodiesel (BD) from an Amazon region oil. The project, involving activities in class and in the laboratory, was given during 8 weeks of the spring semester of 2022. The students were asked about their previous contact with the synthesis and…

Calorimetry is a central concept in the first semester general chemistry curriculum, and constant pressure (coffee-cup) calorimetry is a common experiment in the laboratory. However, constant volume (bomb) calorimetry is traditionally reserved for the physical chemistry laboratory. This article describes the advantages of incorporating bomb…

Ultraviolet (UV)-visible (Vis) spectroscopy is widely used in all modern laboratories as a routine method of analysis. The monitoring of chemical reactions in an aqueous solution involving a gas product is a demanding task but particularly for oscillatory reactions which are obtainable in a narrow concentration range. In this work, the…

This study presents a low-cost Arduino-based gas chromatography system that is suitable for teaching analytical chemistry in an undergraduate laboratory. The gas chromatography system is built with commonly available materials with a total cost less than $100. A Python code is also provided as a user interface that will record data and display the…

Trace metals when present in crude oil or fuels are of economic significance in refining and to the combustion engines that use them. Herein, we develop a laboratory activity that trains students on how to analyze crude oil samples for ash and trace metal content while giving them the opportunity to acquire skills needed as a quality control…

Many students may not be aware that renewable biological materials can be converted into multiple bioproducts and biofuels using a biorefinery process, a more sustainable alternative to conventional crude oil refineries. By using waste from pineapple, a plant material that most students are familiar with, a biorefinery can be modeled to…

Thermal conductivity is generally the tool of choice for quantification of fixed gases, particularly lighter-than-air gases. Unfortunately, gas chromatography-thermal conductivity detectors (GC-TCDs) are difficult to introduce in first- and second-year chemistry courses where the cost and number of instruments, as well as the space required, is…

Biodiesel is an important biomass, largely employed in the transport sector and produced from vegetable oils. Additionally, waste cooking oils may be reused to produce biodiesel fuel, minimizing environmental pollution. A laboratory experiment that affords a widespread way to discuss degradation concepts and tools for used vegetable oil…

Technology and validation methods for producing biodiesel have been updated and have kept advancing. Creative raw materials used in producing environmentally friendly biodiesels have also attracted interest from scientists. Thus, learning and teaching methods on biodiesel production at the high school level need to be up to date. However, there…

Biodiesel is an important alternative fuel synthesized by the trans-esterification of vegetable oils, animal fats, and recycled greases. In this experiment, students prepared biodiesel through the base-catalyzed trans-esterification of several vegetable oils, which were subsequently analyzed in comparison with conventional petroleum-based fuels to…

A modular experiment for upper-level undergraduate students is presented, featuring the product cycle and process evaluating the quality and quantity of biodiesel obtained from a microalgae feedstock grown under carbon-supplemented and nutrient-deprived conditions. Batch reactors are used to cultivate and harvest microalgae, which undergo…

A safe, convenient, and environmentally benign laboratory experiment for the synthesis of biodiesel from six kinds of vegetable oils has been developed for the introductory organic chemistry laboratory. The experiment uses ultrasonic irradiation in the presence of a base catalyst at room temperature and atmospheric pressure. Because of safer and…

This laboratory experiment leverages the pedagogical value and multidisciplinary nature of biodiesel production from vegetable oil to introduce students to continuous-flow chemistry, a modern and rapidly growing approach to chemical synthesis. An interdisciplinary approach exposes students to the practical and conceptual aspects of modern…

An experimental procedure is presented that was developed by fifth-year chemical engineering and industrial chemistry undergraduates at the Federal University of Rio de Janeiro doing the discipline on Experimental Organic Technology. The aim of this study was to apply the solvatochromic effect of the dye Nile Blue chloride to the characterization…

Universities play an important role in society. On the other hand, more and more governments and international organizations are concerned about the environment. Thus, both in their educational programs and research, as well as in the case of public exhibitions, universities are increasingly including subjects related to the environment and its…