In this laboratory experiment, students performed thermogravimetric analysis (TGA) coupled with mass spectrometry (MS) of herbaceous materials (TGA-MS) and learned to analyze mass-loss curves, as well as identify common fragmentation ions. The experiment is the first one to present the application of TGA in a currently relevant topic: biomass…

Experiments are described that involve undergraduates learning concepts of nanoscience and chemistry. Students prepare nanopatterns of organosilane films using protocols of particle lithography. A few basic techniques are needed to prepare samples, such as centrifuging, mixing, heating, and drying. Students obtain hands-on skills with nanoscale…

Lab-on-a-chip technology is brought into the classroom through development of a lesson series with hands-on practicals. Students can discover the principles of microfluidics with different practicals covering laminar flow, micromixing, and droplet generation, as well as trapping and counting beads. A quite affordable novel production technique…

Carbon nanomaterials have promising utility in chemical sensing including applications in preserving occupational safety, monitoring of environmental pollution, and human health. While recent advances in device fabrication and molecular design of functional materials have enabled rapid fabrication of chemical sensors from carbon nanomaterials,…

This paper describes a laboratory exercise that provides students enrolled in introductory nanotechnology courses with an opportunity to synthesize polymer structures with micro- and nanoscale dimensions. Polyvinylpyrrolidone (PVP) films deposited on corrugated PDMS stamps using student-built spin coaters were transferred to clean, dry substrates…

Rania Gikopoulou is a primary school teacher and post-doctoral researcher at the National and Kapodistrian University of Athens. In this article she describes how her 5th grade class (Age 11) learned about abstract phenomena through models of their microscopic structure.

Measuring the heat capacity ratios, [gamma], of gases either through adiabatic expansion or sound velocity is a well established physical chemistry experiment. The most accurate experiments depend on an exact determination of sound origin, which necessitates the use of lasers or a wave generator, where time zero is based on an electrical trigger.…

The rapid academic and industrial development of nanotechnology has led to its implementation in laboratory teaching for undergraduate-level chemistry and engineering students. This laboratory experiment introduces the galvanic replacement reaction for synthesis of hollow metal nanoparticles and investigates the optical properties of these…

A 45 MHz benchtop NMR spectrometer is used to identify the structures and determine the amount of 1-bromoethylbenzene and 1,1-dibromoethylbenzene produced from free-radical bromination of ethylbenzene. The experiment is designed for nonchemistry majors, specifically B.S. Biology students, in a predominantly undergraduate institution with…

The siphon is a very useful example of early technology, the operation of which has long been well understood. A recent article makes the claim that established beliefs regarding this device are incorrect and proposes a "chain model" in which intermolecular forces within the fluid play a large role while atmospheric pressure does not. We have…

Used since the time of the ancient Egyptians as a method for transferring liquids from one vessel to another, the siphon is a dependable tool. Although, the act of siphoning beer from a fermentation barrel or wine from a demijohn is a skill that has been passed down from generation to generation, do we really know how the siphon works? It is…

The Young-Feynman two-hole interferometer is widely used to present electron wave-particle duality and, in particular, the buildup of interference fringes with single electrons. The teaching approach consists of two steps: (i) electrons come through only one hole but diffraction effects are disregarded and (ii) electrons come through both holes…

Millikan's oil-drop experiment is one of the classic experiments from the history of physics. Due to its content (the determination of the elementary charge) it is also among those experiments that are frequently used and discussed in teaching situations. Disappointingly, a review of the educational literature on this experiment reveals that its…

An experiment analogous to that devised by Grimaldi and subsequently repeated by Young to study the nature of light has been realized with electrons. Following the Grimaldi and Young line of thought, an original approach is presented to introduce undergraduate physics students to the wave behaviour of electrons. An electron microscope equipped…

In this article, we studied the microwave permittivity of the complex of the single-walled carbon nanotube and paraffin in 2-18GHz. In the range, the dielectric loss of single-walled carbon nanotube is higher, and the real part and the imaginary part of the dielectric constant decrease with the increase of frequency, and the dielectric constant…