The Folch method is a commonly employed, simple biochemical procedure used to extract fat from food items and biological samples in biochemistry laboratories. The iodine number of fat reflects its degree of unsaturation. In the present study, the iodine number of fat extracted using the Folch method from cow milk, goat milk, chicken egg yolk and…

This article reports the results of a curriculum survey of 322 analytical chemistry instructors (92% U.S.-based) conducted during Spring 2021. This snapshot of current course formats, topics, and pedagogical methods will be useful to both seasoned and novice teachers of analytical chemistry. The majority of respondents reported that their major…

A structured inquiry experiment for inorganic synthesis has been developed to introduce undergraduate students to advanced spectroscopic techniques including paramagnetic nuclear magnetic resonance and electron paramagnetic resonance. Students synthesize multiple complexes with unknown first row transition metals and identify the unknown metals by…

A differential scanning calorimeter was used to study homogeneous nucleation of ice from micron-sized aqueous ammonium sulfate aerosol particles. It is important to understand the conditions at which these particles nucleate ice because of their connection to cirrus cloud formation. Additionally, the concept of freezing point depression, a topic…

Experiments are described for the reliable small-scale glovebox preparation of CpMo(CO)[subscript 3](CH[subscript 3]) and acetyl derivatives thereof through phosphine-induced migratory insertion. The robust syntheses introduce students to a variety of organometallic reaction mechanisms and glovebox techniques, and they are easily carried out…

Systematic errors can cause measurements to deviate from the actual value of the quantity being measured. Faulty equipment (such as a meterstick that is not marked correctly), inaccurate calibration of measuring devices (such as a scale to measure mass that has not been properly zeroed), and improper use of equipment by the experimenter (such as…

Gerald Rutherford (1964), one of the original authors of the Harvard Project Physics course which emphasized the history of science, expressed a view of inquiry which advocated the historical re-constructions of significant experiments. To implement this view we examine two modes of historical re-constructions; Heering's ("Paper…

The creative application of low-cost, readily available materials and techniques promotes inclusion and provides accessibility in the classroom and laboratory for students who are blind or have low vision. Difficulties encountered by these students include operation of laboratory equipment, execution of ordinary laboratory procedures, and use of…

Describes a laboratory exercise containing a practical series of experiments that novice students can perform within two hours. The exercise provides a confirmation of van't Hoff's law while placing more emphasis on osmotic flow than pressure. Students can determine parameters such as the reflection coefficient which stress the interaction of both…

The various equipments, procedure and hazards in constructing the device for inflating a methane balloon using a standard methane outlet in a laboratory are described. This device is fast, safe, inexpensive, and easy to use as compared to a hydrogen gas cylinder for inflating balloons.

Provides background information, apparatus needed, and procedures for an experiment to measure transient response of a stirred vessel. The inexpensive apparatus can be used for two different experiments, reducing cost per experiment. Both experiments use salt dilution as the method of demonstration. (Author/JN)

Describes some experiments for investigating the speed of atomic gas beams and displaying their atomic character. Discusses the experimental apparatus and the time-of-flight method. (YP)

Describes the study of dung-inhabiting or coprophilous fungi to illustrate basic lab techniques and fundamental ecological concepts. Contains 24 references. (WRM)

Discusses the use of two television sets with UHF coverage and a window screen or aluminum foil reflector to conduct a take-home experiment in physics. (CC)

The use of 10cc. syringes in high school chemistry experiments can reduce the expense of equipment and lead to imaginative experimental designs. Describes the equipment and experimental procedures for four experiments utilizing syringes. (JR)