Starting with a double replacement reaction in alcohol between Ni(H[subscript 2]O)[subscript 6](NO[subscript 3])[subscript 2] and NaX, students exploit solubility differences to produce a solution of NiX[subscript 2] and a NaNO[subscript 3] precipitate. They then synthesize a bis(N,N-diethylethylenediamine) Ni(II) complex with chloride, bromide,…

An undergraduate laboratory experiment has been developed for the synthesis of a reactive cross-linker that is useful in various highly visual demonstrations of organic reactivity, click chemistry, and biobased polymer synthesis. A triazolinedione-based cross-linker, which is known as a useful reagent for click chemistry, can be obtained from…

Removing the pollutants from various wastewater is crucial to the environment, ecology, and humans. However, the pollutants are generally removed by chemical decomposition, which not only consumes a lot of energy but also produces carbon emissions. Electrochemical flocculation is effective to extract pollutant molecules and heavy ions from…

Instruction in quantum mechanics is becoming increasingly important as the field is not only a key part of modern physics research but is also important for emerging technologies. However, many students regard quantum mechanics as a particularly challenging subject, in part because it is considered very mathematical and abstract. One potential way…

There is a growing need for chemistry students to be able to handle and manipulate large datasets and analyze them in an efficient and accessible way. This creates the need to develop course materials that introduce these topics early in the undergraduate curriculum. To address this growing need, this activity introduced RStudio to students…

Fluorescence experiments hold great potential to develop and deepen student understanding of fundamental chemical concepts because the phenomenon is engaging and also illustrates many different chemical concepts and applications, including in quantum mechanics, spectroscopy, kinetics, equilibrium, and stoichiometry, through easily observable…

A multioutcome, discovery-based column (CC) and thin layer chromatography (TLC) experiment has been designed for introductory organic chemistry. Multiple outcomes were established using commercially available two- and three-component analgesic medications based on acetaminophen, acetylsalicylic acid (aspirin), and ibuprofen. A series of 11…

A one-pot multicomponent synthesis of unsymmetrical indole-substituted methane derivative based on two consecutive reactions of p-methylbenzaldehyde with N-methylindole and 5,5-dimethyl-1,3-cyclohexanedione is described as an experiment that was carried out by second-year undergraduate chemistry students individually in a laboratory classroom. The…

A procedure to purify anthocyanin, a natural pigment, following a green approach by using macroporous resin and its encapsulation for the maintenance of its stability is described. This laboratory experiment, which describes the benefits of using resin for the purification, is a learning tool for students working in the field on nutraceuticals.…

A single-slit diffraction experiment in an introductory physics laboratory is generally comprised of a rectangular slit and a laser source. The laser beam is sent to the slit producing the well-known diffraction pattern on the screen. This paper proposes a simple modification of the single-slit diffraction experiment to increase student attention…

NMR spectroscopy is a powerful spectroscopic tool that not only allows the determination of structures after synthesis, as usually explained to students of Organic Chemistry, but also is useful in many other fields such as medicine imaging, real-time industrial processes, material sciences, or metabolomics. In this experiment, students performed a…

We propose a laboratory experiment on the quantitative study of the normal dispersion of light. A triangular isosceles prism made of flint glass TF3 is used as the object of study, and we describe a simple and affordable device for observing and photographing the dispersion spectrum on a smartphone. A possibility of the quantitative investigation…

A 2.7 m long stringless pendulum was set up to measure the coefficient of rolling friction of various balls, at higher rolling speeds than usually observed with a short stringless pendulum. The arrangement is easy to set up and makes an impressive classroom demonstration as well as an interesting laboratory experiment.

Calculating analytical uncertainties as a part of method validation is a relevant aspect of field and laboratory practices in instrumental analytical chemistry subjects, which usually require complex algorithms. This work describes the development and didactic use of an automatic and straightforward informatics tool, implemented in an Excel macro,…

Background: The adoption of virtual laboratories (VLs) has experienced a significant surge, catalysed by the global changes in the educational landscape, notably influenced by the COVID-19 pandemic. Originally supplementary to traditional in-person laboratory experiments, VLs swiftly transitioned into a primary source of hands-on laboratory…