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Newman, Karla – Journal of Chemical Education, 2018
Almost all commercial quadrupole ICP-MS instruments use collision/reaction cells to either attenuate spectral interferences or shift the analyte of interest to an interference-free "m/z" (e.g., by O addition). A laboratory practical was developed to introduce the students to the basic operating principles of ICP-MS using a hands-on…
Descriptors: Molecular Structure, Spectroscopy, College Science, Laboratory Experiments
Angelo, Nicholas G.; Henchey, Laura K.; Waxman, Adam J.; Canary, James W.; Arora, Paramjit S.; Wink, Donald – Journal of Chemical Education, 2007
An experiment for the undergraduate chemistry laboratory in which students perform the aldol condensation on an unknown aldehyde and an unknown ketone is described. The experiment involves the use of techniques such as TLC, column chromatography, and recrystallization, and compounds are characterized by [to the first power]H NMR, GC-MS, and FTIR.…
Descriptors: Organic Chemistry, Laboratory Experiments, Inquiry, Undergraduate Students
Fenk, Christopher J.; Kaufman, Nathan; Gerbig, Donald G., Jr. – Journal of Chemical Education, 2007
A new, fast and effective colorimetric analysis of the artificial sweetener aspartame is presented for application in undergraduate laboratory courses. This new method incorporates the use of a modified biuret reagent for selective detection and analysis of aspartame in aqueous solutions. The modified reagent is less caustic than the traditional…
Descriptors: Undergraduate Study, Chemistry, Laboratories, Undergraduate Students