The measurement of glucose through electrochemical methods is a great example to illustrate the practical application of electrochemistry. Although many students enrolled in chemistry classes are familiar with the glucose meter, only a few have delved into the underlying principles governing its operation. This experiment aims to address this gap…

The amount of protein in complex matrices such as food products is an important characteristic, at both a nutritional and a pedagogical level. There are several methods available for protein quantification, from simple UV absorption to mass spectrometry. The most common are based on the interaction of the proteins with colored compounds followed…

SSurfactants or surface-active agents are interesting groups of compounds with characteristic structures, allowing them to decrease the surface tension. A surfactant consists of a hydrophilic head and a hydrophobic tail. Typically, surfactant molecules aggregate into micelles at the critical micelle concentration. In this work, the concept of…

In this paper, a problem set activity focused on understanding and applying unsupervised and supervised chemometric methods for the analysis of biodiesel-diesel blended fuels is described. This problem set was utilized in two upper-level analytical elective courses aimed for junior and senior level students. The data set consists of peak areas…

Organic electrode materials are progressively becoming a research hotspot for energy storage materials due to their renewable and environmentally friendly features. Inspired by the energy transduction mechanism of flavin adenine dinucleotide (FAD) on the inner mitochondrial membrane of living organisms, the lithium storage electrochemical behavior…

Pulsed field gradient nuclear magnetic resonance (NMR) is used to estimate the size of quantum dots (QDs) produced in a simple, fast, small-scale synthesis. This upper-division laboratory experiment teaches the basics of QD synthesis and pulsed field gradient NMR, a powerful technique for measuring diffusion coefficients in solution. The diffusion…

There is an increasing need for fundamental electrochemistry concepts to be taught in the undergraduate curriculum, given the broad applicability of electrochemical technologies in addressing a wide range of global issues from critical energy shortages to real-time medical diagnostics. However, many electrochemical concepts are often taught in…

Fluorescence analysis is an important technology, which can obtain the concentration of target analytes through comparing the fluorescence intensity change of a fluorescent sensor. Generally, the fluorescence intensity is measured by a fluorometer. However, many undergraduates have no chance to operate such an expensive instrument. Besides, the…

Kombucha, a popular probiotic beverage, contains detectable concentrations of ethyl alcohol. To be sold as a nonalcoholic product, alcohol concentrations in kombucha must be shown to be less than 0.5% by volume. This paper describes the use of an inexpensive, commercially available sensor to reliably and accurately measure alcohol concentrations…

Laboratory automation and data science are valuable new skills for all chemists, but most pedagogical activities involving automation to date have focused on upper-level coursework. Herein, we describe a combined computational and experimental lab suitable for a first-year undergraduate general chemistry course, in which these topics are…

Many of the current synthetic methodologies utilized within academic and industrial laboratories require knowledge of how to safely handle air- and moisture-sensitive reagents and work under inert atmospheres. As a result, the ACS Committee on Professional Training recommends incorporating synthetic methods that make use of these inert atmospheres…

This laboratory experiment was divided into four parts. In the first part, students evaluate previously published data and check their normality using histograms, Q-Q plots, the Shapiro-Wilk test, and boxplots. In the second part, two different groups were compared. First, data normality and homoskedasticity were checked by using the Shapiro-Wilk…

The pharmaceutical industry relies heavily on analytical techniques for identifying and characterizing drug compounds. In this experiment, undergraduate pharmacy students explored the applications of near-infrared spectroscopy for pharmaceutical analysis and its potential for identifying patterns and relationships among pharmaceutical samples. In…

Student engagement is an important consideration when incorporating active learning activities into a classroom. To facilitate the large-scale assessment of students' engagement in activities, a survey measure must first be developed and evaluated. Therefore, the goal of this study was to create a self-report measure of student engagement for use…

This study aims to evaluate the laboratory safety perception, awareness and attitude of undergraduates toward the chemistry teaching laboratory by means of a self-administered questionnaire. The survey contains a sample size of 959 undergraduates in Tianjin University of Technology involving four schools. Instrument reliability and validity are…