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Direct linkO'Connor, Kenneth J.; Zuspan, Kimberly; Berry, Lonnie – Journal of Chemical Education, 2011
Hydrogenation of alkenes is an important reaction in the synthesis of organic molecules. In this experiment, students conduct a high-yield microscale hydrogenation reaction of methyl "trans"-cinnamate using a readily available, safe, and convenient hydrogen source. The conditions are similar to those seen in an organic chemistry textbook for an…
Descriptors: Reaction Time, Organic Chemistry, Undergraduate Study, College Science
Shell, Thomas A.; Shell, Jennifer R.; Poole, Kathleen A.; Guetzloff, Thomas F. – Journal of Chemical Education, 2011
A microwave-assisted synthesis of "N"-phenylsuccinimide has been developed for the second-semester organic teaching laboratory. Utilizing this procedure, "N"-phenylsuccinimide can be synthesized in moderate yields (40-60%) by heating a mixture of aniline and succinic anhydride in a domestic microwave oven for four minutes. This technique reduces…
Descriptors: Reaction Time, Organic Chemistry, Science Laboratories, Science Instruction
