A laboratory experiment has been devised to train new graduate trainees in the safe and controlled handling of air-sensitive organometallic reagents using Schlenk lines, high vacuum pumps, liquid nitrogen traps, and cannula transfers. The reaction involves the formation of air-, moisture-, and thermally sensitive 2-pyridyllithium, generated in…

The glowing discharges of plasma obtained by introducing direct current high voltages between two electrodes in a chamber that contains a low pressure gas produces a spectacular effect that makes it attractive to be used as a laboratory experiment for students. Setting up this experiment is however costly and has crucial safety issues to be…

An operationally straightforward, project-like laboratory experiment has been developed in which students directly compare the reactivity of two heterocycles, a cyclic "O,O"-acetal (standard C-O protecting group) and a cyclic "N,O"-acetal (oxazolidine), toward sodium borohydride and methylmagnesium iodide. Students synthesize a…

Water exhibits a maximum in density at normal pressure at around 4° degree temperature. This paper demonstrates that during cooling, at around 4 °C, the temperature remains constant for a while because of heat exchange associated with convective currents inside the water. Superficial approach implies it as a new anomaly of water, but actually it…

One dimensional (1-D)[superscript 1] H and [superscript 13]C NMR experiments are common tools used in undergraduate organic laboratories to characterize synthesized molecules. However, 1-D NMR spectra cannot always provide unambiguous structure determination. In research laboratories, advanced NMR spectroscopy methods are employed for structural…

A well known physics problem is to calculate the friction forces required to support a ladder against a wall. A more tractable problem is to calculate the friction forces needed to support an inclined beam on a ball or a cylinder. In the latter case there are three rather than two points of sliding support. Measurements and calculations are…

The impact force and duration when one billiard ball collides head-on with another is estimated by assuming that the balls are connected by a spring. The results are compared with a measurement when a billiard ball collides with a heavy, rigid surface.

In a traditional teaching approach, a physics course begins with mechanics, and generally the braking effect due to magnetic interactions is not mentioned among the various types of friction presented (static, sliding, rolling) because students will discover magnetism only in later chapters. In our didactic experience this traditional choice is…

The article describes research work that can help students observe and experimentally research the effects caused by the emission component of the filament current in fluorescent lamps' cathodes. When analysing the work of electronic devices--multi-purpose lamps that use thermionic emission--research usually focuses on the current caused by the…

A method is described to measure the coefficient of restitution (COR) by dropping a ball on a piezoelectric disk. Multiple bounces can be observed at small drop heights, so the average COR over say ten bounces can be obtained from just one ball drop, without having to measure the bounce height or the bounce speed. The results show directly that…

A flash purification system using prepacked cartridges containing different silica weights and particle sizes was employed to demonstrate the influence of column characteristics on chromatographic resolution. This chromatographic experiment was a helpful introduction to chromatographic courses where the influence of particle sizes was addressed…

Smartphones and their internal sensors offer new options for an experimental access to teach physics at secondary schools and universities. Especially in the field of mechanics, a number of smartphone-based experiments are known illustrating, e.g., linear and pendulum motions as well as rotational motions using the internal MEMS accelerometer and…

A two to three period analytical chemistry experiment has been developed which allows second year students to explore chemical color tests used to detect adulterated pharmaceuticals. Students prepare several paper analytical devices (PADs) to generate positive and negative controls antibiotics, along with cutting agents such as starch and chalk.…

When the COVID-19 pandemic forced school closures, science, technology, engineering, and mathematics (STEM) teachers were left with the challenging task of devising ways for students to conduct experiments at home. This was necessary because experiments and other hands-on activities are integral to STEM education and are linked to the development…

In science class, students learn by making and living information, enabling them to make sense of knowledge effectively and permanently and to associate it with daily life. Applied science courses make learning more qualified. While science teaching is carried out in application areas such as laboratories, virtual laboratories are used with the…