Discusses the need to encourage increasing numbers of persons to enter analytical chemistry, educate them thoroughly in basic chemical science, and expose them to the most modern methods and instrumentation. Examines some problems and several university's efforts to overcome them. (MVL)

Described is an experiment to investigate the plasticizer content in polyvinyl chloride (PVC) products. The experiment is designed for college students using an instrumental analysis laboratory. (RH)

Describes a learning project in analytical chemistry in which students are required to select instruments from the manufacturers' literature that would be suitable for a given analytical problem. Several examples are given. (SA)

For colleges/universities, rapid instrument development poses a dilemma, since laboratory teaching instruments rapidly become obsolete and money available for replacing them is dwindling. Discusses role of sophisticated computer simulations, nontraditional educational materials, and part-time work-study opportunities as possible solutions to the…

Describes a laboratory experiment designed to encourage laboratory cooperation among individual undergraduate students or groups. Notes each student contributes results individually and the exchange of data is essential to obtain final results. Uses the polarographic method for determining complex metal ions. (MVL)

Highlights several analytical techniques that are being used in state-of-the-art clinical labs. Illustrates how other advances in instrumentation may contribute to clinical chemistry in the future. Topics include: biosensors, polarization spectroscopy, chemiluminescence, fluorescence, photothermal deflection, and chromatography in clinical…

Presents the construction aspects of a simple but reliable colorimeter made from locally available components. Notes the absorption range to be 400-750-nm. Lists seven experiments done on the instrument. (MVL)

Identifies the properties and characteristics of supercritical fluids. Discusses the methodology for supercritical fluid chromatography including flow rate, plate height, column efficiency, viscosity, and other factors. Reviews instruments, column types, and elution conditions. Lists supercritical fluid data for 22 compounds, mostly organic. (MVL)

Instructional videocassettes can provide efficient learning about analytical instrument maintenance and usage for scientists and technicians. Advantages of this approach include low cost to consumers, step-by-step instructions, and quality control of training. The programs currently available from three companies selling gas chromatographs and…

Presents a review of research focusing on scattering, elution techniques, electrozone sensing, filtration, centrifugation, comparison of techniques, data analysis, and particle size standards. The review covers the period 1986-1988. (MVL)

This review is divided into the following analytical methods: ion spectroscopy, electron spectroscopy, scanning tunneling microscopy, atomic force microscopy, optical spectroscopy, desorption techniques, and X-ray techniques. (MVL)

Describes an advanced NMR project that can be done with a 60-MHz continuous-wave proton spectrometer. Points out the main purposes are to give students experience in second-order NMR analysis, the simplification of spectra by raising the frequency, and the effect of non-hydrogen nuclei on proton resonances. (MVL)

Describes a method for using nuclear magnetic resonance to observe the effect of electronegativity on the chemical shift of protons in similar compounds. Suggests the use of 1,3-dihalopropanes as samples. Includes sample questions. (MVL)

Describes a laboratory technique for quantitative analysis of caffeine by an isotopic dilution method for coupled gas chromatography-mass spectroscopy. Discusses caffeine analysis and experimental methodology. Lists sample caffeine concentrations found in common products. (MVL)

Presents a review of articles appealing to forensic practitioners. Topics include: drugs and poisons, forensic biochemistry, and trace evidence. Lists noteworthy books published on forensic science topics since 1986. (MVL)