Calorimetry is a central concept in the first semester general chemistry curriculum, and constant pressure (coffee-cup) calorimetry is a common experiment in the laboratory. However, constant volume (bomb) calorimetry is traditionally reserved for the physical chemistry laboratory. This article describes the advantages of incorporating bomb…

In recent years, solar-powered photocatalytic water splitting for hydrogen production has drawn great attention as a method to supply clean energy and reduce environmental pollution. This approach, driven by solar energy to synthesize hydrogen gas, is completely renewable and can be used to power hydrogen fuel cells to effectively solve the global…

Organizing undergraduates in chemistry, energy engineering, and chemical engineering specialties to participate in an energy transformation experiment can encourage them to think about the impact of human activities on nature and stimulate them to learn more about the topic. This laboratory experiment demonstrates a general approach to the…

One of the most general aims of universities is to respond to the requirements of society. Health and safety are the most important aspects of professional work and play an important role in universities, as there, future professionals are trained for their future professional life. Scientific and technical degrees require adaptation to this…

An important objective of any analytical chemistry course is for students to generate and interpret data from the analysis of complex, real-world samples in order to assess the effectiveness of the analysis method, including the calibration. In this laboratory exercise, students directly compare calibration methods (external standards and standard…

Biodiesel is an important biomass, largely employed in the transport sector and produced from vegetable oils. Additionally, waste cooking oils may be reused to produce biodiesel fuel, minimizing environmental pollution. A laboratory experiment that affords a widespread way to discuss degradation concepts and tools for used vegetable oil…

In the activity described in this communication, the authors present a simple experiment that can be implemented with moderate operational costs and that allows students to acquire the manipulative skills necessary for chromatographic analysis of a familiar fuel that still plays a fundamental role in providing energy for transport of passengers…

A modular experiment for upper-level undergraduate students is presented, featuring the product cycle and process evaluating the quality and quantity of biodiesel obtained from a microalgae feedstock grown under carbon-supplemented and nutrient-deprived conditions. Batch reactors are used to cultivate and harvest microalgae, which undergo…

A safe, convenient, and environmentally benign laboratory experiment for the synthesis of biodiesel from six kinds of vegetable oils has been developed for the introductory organic chemistry laboratory. The experiment uses ultrasonic irradiation in the presence of a base catalyst at room temperature and atmospheric pressure. Because of safer and…

In this laboratory experiment, students performed thermogravimetric analysis (TGA) coupled with mass spectrometry (MS) of herbaceous materials (TGA-MS) and learned to analyze mass-loss curves, as well as identify common fragmentation ions. The experiment is the first one to present the application of TGA in a currently relevant topic: biomass…

Engaging undergraduates in the environmental consequences of fossil fuel usage primes them to consider their own anthropogenic impact, and the benefits and trade-offs of converting to renewable fuel strategies. This laboratory activity explores the potential contaminants (both inorganic and organic) present in the raw fuel and solid waste…

We designed a hands-on laboratory exercise to demonstrate why injecting an aqueous polymer solution into an oil reservoir (commonly known as "polymer flooding") enhances oil production. Students are split into three groups of two to three. Each group is assigned to a packed Hele-Shaw cell pre-saturated with oil, our laboratory model of…

In this paper, we describe an experiment for the undergraduate physical chemistry laboratory in which students determine the speed of sound in the gases He, N[subscript 2], CO[subscript 2], and CF[subscript 3]CH[subscript 2]F. The experimental apparatus consists of a closed acrylic tube containing the gas under study. White audio noise is injected…

Nanotechnology allows the synthesis of nanoscale catalysts, which offer an efficient alternative for fuel cell applications. In this laboratory experiment, the student selects a cost-effective anode for fuel cells by comparing three different working electrodes. These are commercially available palladium (Pd) and glassy carbon (GC) electrodes, and…

Plants can store the chemical energy required by their developing offspring in the form of triglycerides. These lipids can be isolated from seeds and then converted into biodiesel through a transesterification reaction. This second-year undergraduate organic chemistry laboratory experiment exemplifies the conversion of an agricultural energy…