Reported herein is a multidisciplinary laboratory experiment for advanced undergraduate students that includes elements of material synthesis, in the synthesis of cyclodextrin-containing metal-organic frameworks (CD-MOFs), and environmental chemistry, in the use of these MOFs for pollutant removal. This multiday laboratory experiment starts with…

In this organic chemistry laboratory experiment, students are guided through a series of exercises to understand the behavior of compounds during liquid-liquid extraction. Aspects of density, structure, solubility, acid-base theory, and pK[subscript a] are all incorporated into activities that students complete in groups. After using their initial…

This paper presents an experiment in which students determine the mass sensitivity of three crystal quartz resonators, designed to be carried out in "Physics Laboratory II" at the Institute of Experimental Physics, University of Wroclaw. The authors discuss the process of setting up the experiment and the results of the measurements.…

Anaerobic metabolism is recruited in vertebrates under conditions of intense exercise or lowered environmental oxygen availability (hypoxia), typically resulting in the accumulation of lactate in blood and tissues. Lactate will be cleared over time after the reoxygenation of tissues, eventually returning to control levels. Here, we present a…

To overcome students' inaccurate prior knowledge on primary additive colours, a coloured-light mixer has been constructed to enable students to observe directly the colours produced and reach the conclusion by themselves that the three primary colours of light are red, green, and blue (NOT red, yellow, and blue). Three closely packed tiny…

In this paper we analyse the behaviour of a small-scale model of a magnetic levitation system based on the Inductrack concept. Drag and lift forces acting on our prototype, moving above a continuous copper track, are studied analytically following a simple low-speed approach. The experimental results are in good agreement with the theoretical…

Single photons are used for fundamental quantum physics experiments as well as for applications. Originally being a topic of advance courses, such experiments are increasingly a subject of undergraduate courses. We provide interactive screen experiments (ISE) for supporting the work in a real laboratory, and for students who do not have access to…

This experiment was developed as a means of incorporating instrumental analyses into an introductory chemistry laboratory. A two-component solid mixture of caffeine and ibuprofen is separated through a series of solution extractions and precipitation and their relative amounts measured. These compounds were chosen because the combination of…

Waste newspaper is pulped with acid and its cellulose is hydrolyzed. The resulting glucose syrup is fermented with yeast and distilled to give ethanol. The experiment highlights the potential of applied chemistry to confront problems of economic importance, that is, the effective utilization of biomass to reduce dependence on non-renewable…

Treatment of phenylacetic acid with 90% HNO[subscript 3] yields a product, I, whose observed melting point is 175-179 degrees C and whose equivalent weight is approximately 226 grams. Treatment of phenylacetic acid with 70% HNO[subscript 3] yields a product, II, whose observed melting point is 106-111 degrees C and whose equivalent weight is…

The aryl sulfonate ester, menthyl N-acetylsulfanilate, is synthesized from N-acetylsulfanilyl chloride and menthol in pyridine, then pyrolyzed (thermally decomposed) at reduced pressure. The volatile (elimination) products of the reaction are analyzed using gas chromatography, and the resulting product distribution is used to determine whether the…

Laboratory exercises, which utilize alkaline phosphatase as a model enzyme, have been developed and used extensively in undergraduate biochemistry courses to illustrate enzyme steady-state kinetics. A bioinformatics laboratory exercise for the biochemistry laboratory, which complements the traditional alkaline phosphatase kinetics exercise, was…

Many physical chemistry lab courses include an experiment in which students measure surface tension as a function of surfactant concentration. In the traditional experiment, the data are fit to the Gibbs isotherm to determine the molar area for the surfactant, and the critical micelle concentration is used to calculate the Gibbs energy of micelle…

The cryophorus dramatically demonstrates the cooling effect of evaporation. This article describes some simple and easy-to-make cryophoruses, ideal for demonstrating evaporative cooling to students at all levels. The most dramatic effects occurred with cyclohexane and benzene, with water generally freezing more slowly. (Contains 4 notes, 2 tables,…

In this lab experiment, screen-printed electrode strips are used to illustrate the essential concepts of electrochemistry, giving students an opportunity to explore metal electrodeposition processes. In the past, metal electrodeposition experiments were seldom included in general chemistry labs because of the difficulty of maintaining separate…