The flue gas from waste incineration power plants contains high-level zinc species that may deactivate the catalyst for selective catalytic reduction (SCR) of nitrogen oxides (NO[subscript x]) with NH[subscript 3]. A comparison experiment was designed to investigate the effect of different types and Zn/Ce molar ratios on the performance of…

This paper reports the quantification of Ca, Mg, and Fe as micronutrients in different vegetables (spinach, sugar beets, and carrots) from raw and processed samples. Simple extraction procedures, titrations, and spectrophotometric analysis were used to determine the amounts of micronutrients before and after cooking. From the obtained results, an…

The COVID-19 epidemic adversely impacted chemical engineering experiments(CEEs). Students underwent online learning, i.e., software simulation of the CEE course, instead of laboratory learning. A questionnaire survey revealed that students exhibited low enthusiasm for online learning, showing that online courses cannot ensure learning quality.…

The electrolysis of water to produce hydrogen is a critical step in many green chemistry processes. The key to the efficiency of water electrolysis is the synthesis of an appropriate electrocatalyst. Three-dimensional (3D) printing is an increasingly important part of many industrial processes. In this study, we propose an efficient laboratory…

During the SARS-2-COVID pandemic our institution sought to continue the teaching and learning of experimental laboratories by designing, assembling, and delivering a microscale chemistry kit to the students' homes. Thanks to this approach students were able to perform [approximately]25 experiments during each one of the Fall 2020 and Spring 2021…

This work presents an outline for a full-quartile design-based learning laboratory-based course suitable for final year Bachelor's students. The course has been run for 5 years in the department of Chemical Engineering and Chemistry. The course attempts to provide a complete laboratory experience for its students, including an authentic research…

An experimental procedure is presented that was developed by fifth-year chemical engineering and industrial chemistry undergraduates at the Federal University of Rio de Janeiro doing the discipline on Experimental Organic Technology. The aim of this study was to apply the solvatochromic effect of the dye Nile Blue chloride to the characterization…

To inspire upper-division undergraduate students to gain a deeper understanding of biorefinery, an experiment related to biofuels and lignin-based sunscreen products from corncob was performed in multiple offerings of a summer-semester class. Specifically, corncobs were pretreated with 1% H[subscript 2]SO[subscript 4] to obtain hemicellulose…

Rapid development in the field of reticular chemistry has allowed scientists ever-increasing control over the design and synthesis of crystalline porous materials. The promise that this field has in the development of next-generation materials for numerous applications (gas storage and separation, catalysis, chemical sensing, electronics) relies…

A Unit Operations Laboratory (UOL) is fundamental to undergraduate chemical engineering education. This article discusses a new course structure for the University of Kansas UOL and details for three new experiments covering the fundamentals of vapor-liquid equilibrium, fluid mechanics, and kinetics. Students apply knowledge from these courses as…

This paper describes an undergraduate laboratory experiment where students study the heating behavior of magnetic nanoparticles in the presence of alternating magnetic fields. Average score on the post-test was 45±12% for students who completed the lab online, versus 43±11% for those doing the activity hands-on. Post-test scores were significantly…

In this work, a laboratory experiment to introduce graduate students to nanotechnology is described. Students prepared poly(lactic-"co"-glycolic acid) (PLGA) nanoparticles using two different synthesis procedures, a single and a double emulsion-solvent evaporation method. The students also performed a physicochemical characterization of…

3D printing technology has an enormous potential to apply to chemical engineering education. In this paper, we describe several designs of 3D printed mesoreactors (Y-shape, T-shape, and Long channel shape) using the following steps: reactor sketching, CAD modeling, and reactor printing. With a focus on continuous plug flow mesoreactors (PFRs, i.d.…

An integrative laboratory study addressing fundamentals of enzyme catalysis and their application to reactors operation and modeling is presented. Invertase, a ß-fructofuranosidase that catalyses the hydrolysis of sucrose, is used as the model enzyme at optimal conditions (pH 4.5 and 45 °C). The experimental work involves 3 h of laboratory time…

Third year chemical engineering undergraduate students at The University of Akron designed and fabricated a heat exchanger for a stirred tank as part of a Chemical Engineering Laboratory course. The heat exchanger portion of this course was three weeks of the fifteen week long semester. Students applied concepts of scale-up and dimensional…