In the field of "hydrogen energy", sodium borohydride (NaBH[subscript 4]) is a potential hydrogen carrier able to release H[subscript 2] by hydrolysis in the presence of a metal catalyst. Our laboratory experiment focuses on this. It is intended for thirdyear undergraduate students in order to have hands-on laboratory experience through…

This paper describes a method for determination of trihalomethanes (THMs) in drinking water via solid-phase microextraction (SPME) GC/MS as a means to develop and improve student understanding of the use of GC/MS for qualitative and quantitative analysis. In the classroom, students are introduced to SPME, GC/MS instrumentation, and the use of MS…

Virtually all modern chemical instrumentation is controlled by computers. While software packages are continually becoming easier to use, allowing for more researchers to utilize more complex instruments, conveying some level of understanding as to how computers and instruments communicate is still an important part of the undergraduate…

A laboratory experiment is described for beginning, nonmajor chemistry students, which allows students to examine the phenomena of fluorescence and chemiluminescence, as well as gain experience in basic organic synthesis. Students synthesize fluorescein and bis(2,4,6-trichlorophenyl) oxalate (TCPO) to explore fluorescence and chemiluminescence by…

A series of Microsoft Excel spreadsheets were developed to simulate the process of separation optimization under isocratic and simple gradient conditions. The optimization procedure is performed in a stepwise fashion using simple macros for an automatic application of this approach. The proposed optimization approach involves modeling of the peak…

This letter comments on the paper "Analysis of Citric Acid in Beverages: Use of an Indicator Displacement Assay" ["J. Chem. Educ." 2010, 87 (8), 832-835 (EJ918557)]. Discrepancies in figures and host:indicator complex behavior are discussed and an alternative experimental protocol presented.

An organic chemistry experiment is described that is based on recent research to elucidate a novel cation-pi interaction between tetraalkammonium cations and propargyl hydrazines. This nonbonded interaction is a key component of the mechanism of ammonium-catalyzed intramolecular cycloaddition of nitrogen to the terminal carbon of a C-C triple bond…

A straightforward synthesis of 2-phenylimidazo[1,2-a]pyridine is described. The reaction is designed to demonstrate to students the preparation of a bridged N-heterocycle, in which the heteroatom occupies a bridgehead position. The product is obtained in moderate to high yield and is highly crystalline. The compound can be purified either by…

This study developed a web-based multimedia assessment system (WMA system) and applied it to science laboratory instruction. The goal was to improve students' knowledge acquisition under science laboratory instruction. The developed system enabled learners to perform self-assessments by responding to multimedia technology test items online. The…

The new approach to teaching science presented by the Next Generation Science Standards (NGSS) warrants training high-quality science, technology, engineering, and mathematics (STEM) teachers to prepare the future STEM workforce. We share the implementation of an energy lesson using a nanoscience approach, well-aligned with the NGSS vision, in a…

The role of practical work in the training of student teachers is central to the development of their future pedagogy and practice. However, not all laboratory based activities give sufficient challenge in the development of both cognitive and practical skills. The activity proposed in this paper helps reinforce an understanding of reaction…

The real power of calculus is revealed when it is applied to actual physical problems. In this paper, we present a calculus inspired physics experiment suitable for high school and undergraduate programs. A model for the theory of the terminal velocity of a falling body subject to a resistive force is developed and its validity tested in an…

The use of science kits is a growing trend in India. The kits provide equipments, apparatus and chemicals in the form of a moving laboratory to use in science classes. This research paper highlights the issues and challenges faced by the Government school teachers of Delhi in India while using science kits during teaching-learning process at upper…

Additions to the popular evaporation rate determination laboratory of alcohol-based hand-rub sanitizers are described here. Significantly, inquiry-driven protocols for formulating hand-rub sanitizers, falling-ball viscometry, and sanitizer efficacy are included. Incorporation of familiar substances ("molecular relevance") enables…

In 1849, Hippolyte Fizeau determined the speed of light in a famous experiment. The idea was to measure the time taken for a pulse of light to travel between an intense light source and a mirror about 8 km away. A rotating cogwheel with 720 notches, that could be rotated at a variable speed, was used to chop the light beam and determine the flight…