An organic chemistry experiment designed for senior undergraduates focuses on bifunctional catalysis, a critical yet often omitted topic at the undergraduate level, but essential for advanced studies in chemistry. By utilization of a tertiary amine-thiourea catalyst in the asymmetric Michael addition reaction, the experiment showcases the…

A renewed experimental procedure for the unknown carbonyl experiment has been developed using hydrazone synthesis, thin layer chromatography (TLC) analysis, and melting point determination to differentiate between structurally similar ketones and aldehydes in undergraduate organic chemistry practical courses. Benzaldehyde, p-tolualdehyde,…

Herein, we present an integrated upper division chemistry laboratory experiment involving the synthesis, characterization, and evaluation of catalytic metal--organic frameworks (MOFs). Experiments are designed to facilitate the solvothermal synthesis and characterize MOFs, including UiO-66, UiO-66-NH[subscript 2], and UiO-66-NO[subscript 2]. The…

University courses are often interconnected; however, the connections between these courses remain unclear to many students. This is particularly important in the field of forensic science since each stage of the investigation, from the crime scene to the courtroom, has significant implications on the outcome of a case and the individuals…

Preparative chromatography is one of the most common and important purification techniques in organic chemistry and is employed in laboratories across the globe. In order to facilitate student proficiency with the method, a unique approach for the separation of estragole, ethyl cinnamate, and cinnamyl alcohol using microscale preparative flash…

Many undergraduate chemistry and biochemistry students pursue careers in healthcare. Biomaterials, designed to harmonize with the complexity of the human body, have become increasingly significant in medicine as implants, drug delivery vehicles and tissue scaffolds. We believe it is essential that undergraduates are exposed to biomaterial…

The assessment of student understanding, and of student reasoning skills more broadly, hinges upon the ability to elicit and interpret student-generated explanations. In practice, however, the explanations that students provide in response to traditional prompts do not always reveal as much about student reasoning as teachers and researchers in…

As an introduction to quadrupolar effects in NMR spectroscopy, students use low field ([superscript 1]H, 60 MHz), benchtop [superscript 13]C NMR spectroscopy to contrast the spin-spin coupling behavior of [superscript 13]C to the dipolar [superscript 1]H and quadrupolar [superscript 2]D in familiar solvents C(H/D)Cl[subscript 3], C(H/D)[subscript…

It is generally accepted that if a course or curricular transformation is to be implemented with fidelity, the users must understand how and why the transformation is different from their current practices and which aspects of the transformation are essential to achieving comparable student learning outcomes. In this article, we provide a detailed…

This laboratory experiment consists of the synthesis of two series of alkaline-earth titanates (calcium-strontium and strontium-barium)to corroborate Vegard's law by obtaining their X-ray diffraction patterns and plotting the lattice parameter versus mole fraction of both cations. This experiment allows students to understand the key concepts in…

An experimental design by combining hydrogel and ethylenediaminetetraacetic acid disodium salt (EDTA) for visually displaying chemical complexation reactions is developed. The Na[superscript +] ions on the [alpha]-l-guluronic acid (G) unit of the sodium alginate molecule undergo an ion exchange with a divalent cation, so that the G units are…

In this work, we introduce high school students to renewable energy through the exploration of the pyrolysis process, focusing on the conversion of lignocellulosic biomass into bio-oil. Students undertake a sequence of straightforward experiments in four sessions, using a handmade reactor and various types of biomasses. Outcomes such as yield…

This paper outlines a comprehensive teaching laboratory course program that centers on titration analysis, a timeless and essential technique in analytical chemistry spanning various disciplines, such as environmental science, medicine, and industry. In these fields, titration analysis is paramount for determining the concentrations of substances…

Chemical thinking is a powerful tool for making sense of the material world and acting on it. But developing competence in chemical thinking may be challenging for students as it varies in several dimensions. This contribution seeks to guide and help chemistry educators in the design of learning experiences that support the development of…

Despite the growing importance of nanomaterials in numerous industries, most undergraduate chemistry students are unlikely to encounter characterization techniques common in the field during their education. Scanning electron microscopy (SEM) is a common technique for materials characterization widely used in careers chemistry students are likely…