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Direct linkWithey, Jonathan M.; Bajic, Andrea – Journal of Chemical Education, 2015
A novel procedure is described where students use COMU [(1-cyano-2-ethoxy-2-oxoethylidenaminooxy)dimethylamino-morpholino-carbenium hexafluorophosphate], as a nonhazardous partner, in the one-pot coupling of a carboxylic acid and amine producing N,N-diethyl-3-methylbenzamide (DEET). Fundamental principles of carbonyl reactivity are understood,…
Descriptors: Organic Chemistry, Undergraduate Students, Introductory Courses, Laboratory Experiments
