This paper reports a laboratorial internship included in the Portuguese Science and Technology promotion program "Internships for Young People in Laboratories (Ciência Viva no Laboratório)", which provided high school students an opportunity to approach the reality of scientific and technological research in a higher education…

A laboratory experiment is described in which a simple characterization of a historical lime mortar is made by the determination of its approximate composition by a gravimetric method. Fourier transform infrared (FTIR) spectroscopy and X-ray diffraction (XRD) are also used for the qualitative characterization of the lime mortar components. These…

A novel procedure is described where students use COMU [(1-cyano-2-ethoxy-2-oxoethylidenaminooxy)dimethylamino-morpholino-carbenium hexafluorophosphate], as a nonhazardous partner, in the one-pot coupling of a carboxylic acid and amine producing N,N-diethyl-3-methylbenzamide (DEET). Fundamental principles of carbonyl reactivity are understood,…

Although vacuum technology is essential to many aspects of modern physical and analytical chemistry, vacuum experiments are rarely the focus of undergraduate laboratories. We describe an experiment that introduces students to vacuum science and mass spectrometry. The students first assemble a vacuum system, including a mass spectrometer. While…

Engineers often measure temperature for a wide variety of applications and assessments. This article describes how STEM educators can use thermometers or temperature sensors to help students understand how heat disperses through fluids, both air and water. It also provides hands-on learning about air and water heating systems. (Contains 4 figures.)

At technical colleges and secondary-level tech schools, students enrolled in basic electronics labs who have learned about diodes that do rectification are used to seeing power diodes like the 1N4001. When the students are introduced to low-power zener diodes and signal diodes, component identification gets more complex. If the small zeners are…

We present an adaptation to an experiment previously published in this "Journal". The experiment was designed to determine the heat capacity ratios of gases by measuring the speed of sound using a modified Kundt's tube. The experiment yielded excellent results for all of the gases and gas mixtures measured. Although elegant in its simplicity, it…

The importance of investigating the sun's interior is discussed. One method for probing the interiors of some pulsating stars is described. The relationship between the sun's solar oscillation frequencies and the sun's solar cycles is discussed. A project to place six instruments around the world to observe the sun's oscillations (GONG) is…

A collaborative research program in auger spectroscopy at the University of Liverpool (England) involved scientists from 12 universities and research groups in 5 European countries and financed with international funds is described. The experience of the collaborators suggests how similar projects might be initiated and managed. (Author/MSE)

The author believes that one of the best ways of educating the student of contemporary and future technology is to use modern devices, instruments, and techniques in an up-to-date college laboratory. Experiments which motivate and which are of interest to the student, the professor, and industry should be used extensively. (Author/TS)

Described is a program in which students learn about spectroscopy and instrumentation to solve a chemical forensic mystery. Infrared and nuclear magnetic resonance (NMR) spectroscopy, refractometry, and chromatographic techniques were used. An example of a mystery case is included. (KR)