An apparatus of the 70s for measuring thermal conductivity in different materials is used to visualize, through an infrared thermal imaging approach, temperature fields and the heat diffusion process. The observed temperature profiles also suggest solid grounds for a fair mathematical modelling of this phenomenon.

In this laboratory experiment, students performed thermogravimetric analysis (TGA) coupled with mass spectrometry (MS) of herbaceous materials (TGA-MS) and learned to analyze mass-loss curves, as well as identify common fragmentation ions. The experiment is the first one to present the application of TGA in a currently relevant topic: biomass…

The goal of this laboratory exercise was for students to understand the concept of chirality and how enantiomeric excess (ee) is experimentally determined using the analysis of ibuprofen as an example. Students determined the enantiomeric excess of the analyte by three different instrumental methods: mass spectrometry, nuclear magnetic resonance…

Reviews experiments performed in a mobile spectroscopy laboratory. (SL)

Reviews a cooperative program in which a number of nearby chemistry departments combined to purchase a mobile spectroscopy laboratory housed in a step-van truck. (SL)

Traces the development of instruments used in spectrophotometry. Discusses how spectrophotometric measurements are made. Describes the color comparator, the filter photometer, and the spectrophotometer. Outlines the evolution of optical systems, including light sources, the monochromator, the photodetector, double-beam optics, and split-beam…