A laboratory experiment was developed to introduce undergraduate chemistry students to the chemical characterization of agroindustrial waste extracts by gas chromatography-mass spectrometry (GC--MS). The students prepared hexane and dichloromethane extracts from black pepper ("Piper nigrum" L.) waste. GC--MS analysis revealed the…

When searching for a known target, mental representations of target features, or templates, guide attention towards matching objects and facilitate recognition. When only distractor features are known, distractor templates allow irrelevant objects to be recognised and attention to be shifted away. This is particularly true in X-ray baggage search,…

Biochemistry is about structure and function, but it is also about data and this is where computers come in. From my time as a graduate student and post doc, whenever I encountered data I thought, "I can work this up by hand, but I think a computer could do a better job." Since that time, I have been working at the interface of…

Marble, formed by the metamorphism of limestone, is commonly used in the construction industry and sculpting. The mineral in marble is either calcite [CaCO[subscript 3]] or dolomite [CaMg(CO[subscript 3])[subscript 2]] or sometimes both. The pure white Carrara marble from Italy was made a household name by Michelangelo, the famous sculptor of the…

Infrared (IR) spectroscopy and catalysis represent two of the most practically relevant topics in chemistry, but they are normally taught in separate contexts at the undergraduate level. Although IR spectroscopy is introduced to students as a tool for organic compound characterization, it also finds wide applicability in the investigation of…

Recently, topical products advertising cannabinoid ingredients have gained popularity. Consumers are seeing an increase of commercial products containing ingredients from hemp oil to cannabidiol (CBD) due to health benefit claims. Cosmetic products containing cannabinoids are currently not regulated at the federal level. A laboratory experiment…

Oxidation reactions are critical components of the synthetic toolbox taught to undergraduate students during introductory organic chemistry courses. However, the oxidation reactions discussed in the undergraduate curriculum are often outdated as many organic chemistry textbooks emphasize chromium-based oxidants that are no longer in regular use by…

Organic chemistry students often struggle with reaction mechanisms, particularly in how they are proposed and justified. In this activity targeting second year organic undergraduates, students used infrared spectroscopy (IR) to track the reaction progress of two distinct aldol reactions and used polarimetry to analyze the stereoselectivity of…

Chemistry in water is an emerging field that fulfills the fifth principle of green chemistry: replacing toxic organic solvents with their benign counterparts. Although some pharmaceutical industries have developed and adopted chemistry in water, its implementation in teaching laboratories is still limited. Therefore, we have designed an experiment…

This work presents a homemade multirole 3D-printed modular spectrometer(MPMS), which can be easily assembled like bricks and expanded with several modules to measure different types of spectra, such as UV-vis absorption, fluorescence emission, flame emission/absorption, glow discharge, and even Raman spectra. The spectrometer is designed to be…

Microplastics have been detected in most ecosystems around the world. They affect the environment and organisms in it, including humans and possibly their health. Hence, the analysis of microplastic occurrence in the environment is highly relevant. However, there are only a few practical and easy-to-implement methods published for school use, and…

We report here a successful adaptation of lab videos used during remote instruction to a kinetics experiment reported in this Journal in 2007. In the in-person lab, students now record their rate data on their cell phone cameras and then collect their data from the videos for their postlab reports; previously, they acquired the data in real time…

A two-component undergraduate laboratory experience has been developed by students in a senior level capstone course. The first component is a 3 h laboratory experience dedicated to the rapid synthesis of a metal-organic framework (MOF-808) in aqueous solution using readily available reagents and equipment. During the second component, MOF-808 was…

A cooperative-learning jigsaw-style activity was developed to create opportunities for introductory organic chemistry students to discuss and decipher [superscript 1]H NMR spectra. Students cooperatively interpreted spectra that contained both pure and mixed solvents, building consensus through explanation and argumentation on what each spectrum…

The laboratory is a complex environment where the three levels of the chemistry triplet coincide. As the laboratory environment places a large demand on the working memory of students, cognitive load theory can address overload which causes barriers to learning. Breaking down barriers requires iterative phases of analysis/exploration,…