Green chemistry is finding its place as one of the most essential study topics in the curriculum of future chemists and chemical engineers. Experiments that meet green chemistry principles contribute to make the laboratory a safer working place, generate less waste, and allow students to increase their knowledge in new environmentally friendly…

Low-dimensional materials especially graphene-based are of high interest to a broad community. One of the most fundamental aspects in the biomedical field is material characterization, which helps understand their property and tune for application. Though the existing teaching curricula are well standardized to include basic principles and…

Few laboratory exercises exist that introduce undergraduate students to both the concepts and instrumentation used in rotational spectroscopy. Because of this gap in undergraduate laboratory training, a teaching laboratory for the pure rotational spectroscopy of benzonitrile has been developed and reported. Owing to benzonitrile's recent discovery…

Triboluminescence is a fascinating phenomenon that can engage students' interest in chemistry. However, safe, cost-effective, and accessible laboratory experiments featuring highly triboluminescent substances are limited. To bridge this gap, we present a simple, rapid, semimicro test tube preparation of the visually engaging manganese complex…

Nitrate is a crucial parameter for assessing water quality, owing to its dual function in ecological systems. These functions can be beneficial or detrimental depending on whether nitrate concentrations are low or high, respectively. The ultraviolet spectrophotometric method (standard as 4500-NO[subscript 3]--B) is a classic method for determining…

Smartphones, coupled with small mobile sensors, make it possible to work with near-infrared (NIR) spectroscopy in science classrooms. NIR spectroscopy has become a standard analytical technology in various industries. These new devices enable students to create their own data in real time. This article presents an inquiry-based teaching unit, in…

A set of inexpensive and pedagogically rich experiments focusing on S[subscript N]1, E1, and E2 reactions have been updated to include modern computational and spectroscopic analyses. The S[subscript N]1 experiment involves treatment of "tert"-amyl alcohol with hydrochloric acid to generate the corresponding alkyl chloride, which is used…

In this guided-inquiry lesson, students were tasked with determining the efficacy of an at-home drinking water filter at removing lead (Pb) from tap water using graphite furnace atomic absorption spectroscopy by determining the concentration of lead before and after filtration. The lesson was structured to allow students to choose and perform…

The Spring 2020 semester students were faced with the challenge of adjusting how they learned in the middle of the semester, as the situation changed from instructors holding group office hours and study sessions for the upcoming midterm exams to faculty and students scrambling to gather their belongings before the impending lockdown. Immediately…

The importance of utilizing spectroscopic techniques for unraveling structural and compositional changes in nonreacting and reacting systems is unquestionable. Nowadays, efforts are directed towards the introduction of relevant spectroscopic techniques to undergraduate students in order to prepare them for future careers in industry and academia,…

Chemistry undergraduate curricula typically place Nuclear Magnetic Resonance (NMR) lectures under either Organic Chemistry or Spectroscopy courses, aiming for students to acquire basic knowledge for the determination of the structure of simple organic compounds. On the other hand, regarding laboratory practice, NMR is frequently disregarded by…

Inorganic phosphors are the main component of light emitting diodes which have caused the revolution in lighting industry as an energy-efficient and long-lasting replacement of traditional incandescent light bulbs and fluorescent tubes. They are also used in various consumer products and displays and can potentially find applications in…

Students learned the principles and practice of photometry through project-based learning. They addressed the challenge of measuring the unknown concentration of a colored substance using a photometer they were required to design, build, and test. Then, they used that instrument to carry out the experiment and fulfill the challenge. A photometer…

The laboratory is a complex environment where the three levels of the chemistry triplet coincide. As the laboratory environment places a large demand on the working memory of students, cognitive load theory can address overload which causes barriers to learning. Breaking down barriers requires iterative phases of analysis/exploration,…

Fractional distillation is part of the essential experimental techniques taught to first-year chemistry students, especially during practical organic chemistry work. The characterization of the distillate generally involves measuring the boiling temperature, the refractive index, or the infrared spectrum. In this paper, an unknown mixture composed…