Metal-organic frameworks (MOFs) are a class of porous materials that are often crystalline with high surface area and structural tunability. In this laboratory experiment designed for inorganic chemistry students at the undergraduate level, students complete a two-step experiment where they will first (i) synthesize two isostructural…

The substitution of carbonyl compounds with liquid bromine as a brominating agent is the most commonly employed synthesis method for a-bromoacetophenone and its derivatives. However, liquid bromine possesses certain drawbacks, such as volatilization, high toxicity, strong corrosion, and poor reaction selectivity, which limit its application and…

The process of method development is at the heart of analytical chemistry, yet direct experimental experience with the process is rarely taught in the undergraduate laboratory. We report here an experiment that uses rapid, safe, and inexpensive paper-based microfluidics with cell phone detection in order to facilitate the development of a…

This study's general theme revolves around practical work in chemical education, and its scope is the employment of a novel inquiry strategy combined with a new openness level. We investigate how the controlled positive error, a new device for inquiry activities developed by us, affects undergraduate students' experience of an experiment and…

A set of inexpensive and pedagogically rich experiments focusing on S[subscript N]1, E1, and E2 reactions have been updated to include modern computational and spectroscopic analyses. The S[subscript N]1 experiment involves treatment of "tert"-amyl alcohol with hydrochloric acid to generate the corresponding alkyl chloride, which is used…

This paper presents an insight on the pedagogy and strategic design of the organization of the four experimental subjects of the Chemical Engineering Degree Curricula at the Universidad Politécnica de Madrid (GIQ-ETSII-UPM). Outcome-based learning is applied, focused on the student's work, centering explicitly in Experimental Design outcomes.…

Undergraduate laboratory courses, owing to their larger sizes and shorter time slots, are often conducted in highly structured modes. However, this approach is known to interfere with students' engagement in the experiments. To enhance students' engagement, we propose an alternative mode of running laboratory courses by creating some…

A classic undergraduate introductory experiment is to measure the diffraction and interference pattern from single and double slits to determine slit width and separation. Studies show that Course-based Undergraduate Research Experiences (CUREs) can make science more inclusive when offered at the undergraduate level. Additionally, CUREs help…

Earth's field nuclear magnetic resonance (EFNMR) spectroscopy offers students a unique opportunity to consolidate their understanding of NMR spectroscopic theory through hands-on practice with a simple spectrometer. A comprehensive, 6 h experiment is presented for the introduction of low-field NMR techniques, covering spectroscopy, relaxivity, and…

Teaching emulsion polymerization is an important benchmark in undergraduate polymer courses. However, the introduction of hands-on experiments in undergraduate polymer laboratories is challenging: experimental time, reagents, and equipment involved are the primary restraints. We report a practical emulsion polymerization laboratory experiment for…

The stated purpose of this paper is to provide a simple and quick method to assemble pH electrodes using readily available materials. The present assembled electrodes are comparable with commercial pH electrodes, with accuracy for pH determination in the range 2-12. Furthermore, the constructed simple pH electrodes exhibit a fast and stable…

The CRISPR/Cas9 system is a powerful tool for gene editing and it has become increasingly important for biology students to understand this emerging technique. Most CRISPR laboratory teaching modules use complex metazoan systems or mammalian cell culture which can be expensive. Here, we present a lab module that engages students in learning the…

Flavonoids have been studied extensively for their antioxidant properties. Specifically, the flavonoids in tea, such as catechin and epigallocatechin gallate, have been shown to have positive health effects. These compounds are also oxidizable, so the concentrations of these compounds in a given kind of tea can be determined using cyclic…

A remote experiment was developed and carried out to create a phenol/water phase diagram using a low-cost automated data collection system and an online video broadcast. Both the data and video from the experiment were transmitted in real-time. The remote lab experiment was evaluated using qualitative and quantitative questionnaires filled out by…

A set of biochemistry experiments based on the technique of protein colorimetry is described. Students used the Biuret and Bradford assays to qualitatively and quantitatively assess solutions for protein. Two unique features of these experiments are (1) the use of intentional discrepancies within each experiment to promote critical thinking and…