Liquid metals are widely applied in various fields, including chemistry, catalysis, energy storage, chemical sensing, and stretchable electronics, due to their unique deformabilities. However, their behavior under a rod or ring electrode has never been analyzed. Furthermore, research on the deformation behavior of eutectic Ga--In (EGaIn), the most…

The variation in the transference number of H[superscript +] (aq) is investigated for different HCl solution concentrations. The method for scribing graduations on electromigration tubes is modified to decrease the error in experimental measurements, and metallic copper is used as the anode to reduce the toxicity and environmental impact of the…

As a rule, an experiment carried out at school or in undergraduate study courses is rather simple and not very informative. However, when the experiments are to be performed using modern methods, they are often abstract and difficult to understand. Here, we describe a quick and simple experiment, namely the enzymatic characterization of ptyalin…

Photochemical reactions are initiated by the absorption of light, triggering the chemical reactions and resulting in the formation of products. These reactions are generally performed using a freely available renewable source of energy-solar energy. Solar simulators mimic both the ultraviolet and visible regions of sunlight and hence can serve as…

A laboratory experiment that involves the aqueous and solid phase synthesis, characterization, and solvatochromic properties exploration of red complex [Ni(Me[subscript 3]en)(acac)]BPh[subscript 4] has been developed for first-year undergraduates in the College of Chemistry and Chemical Engineering at Xiamen University. In contrast to previously…

The addition of a small excess of triethyl orthoformate to an alcoholic mixture of NiCl[subscript 2]·6H[subscript 2]O and triphenylphosphine (PPh[subscript 3]) results in an increase in the typical isolated yield of [NiCl[subscript 2](PPh[subscript 3])[subscript 2]] from below 50% to over 85%. The impact of water when present in the reaction…

Short chain fatty acids (SCFAs) are produced in the gut as a result of microbial action on ingested dietary fiber and have been associated with several health benefits. Herein an undergraduate student experiment that uses gas chromatography equipped with either a flame ionization detector or mass spectrometer for the analysis and quantitation of…

Electrochemistry is taught in most undergraduate chemistry programs. Although this topic is important for students due to its broad interest in industry (energy, diagnostics, car industry, etc.), they often find it difficult, because it is based on a combination of various physical concepts such as electric fields, interfacial processes or charge…

A discovery-based experiment for the synthesis of arylpropiolic acids via carboxylation of arylacetylenic Grignard reagents was developed. This experiment shows the "dual utility" of Grignard reagents. In the synthesis of arylpropiolic acids reported here, we have demonstrated the use of a Grignard reagent as a base in a "Grignard…

An undergraduate laboratory experiment has been developed for the synthesis of a reactive cross-linker that is useful in various highly visual demonstrations of organic reactivity, click chemistry, and biobased polymer synthesis. A triazolinedione-based cross-linker, which is known as a useful reagent for click chemistry, can be obtained from…

The trajectory of a ball rolling across an inclined plane was recorded on video film to determine if it followed a parabolic path as others have suggested. The challenges in this case were (a) to determine the magnitude and direction of the friction force on the ball, (b) to determine the effect of the friction force on the trajectory and (c) to…

Blue (B), yellow (Y), red (R), and green (G) color-changing dye was used in a general chemistry course for first-year undergraduate students with nonscience majors to highlight the redox reactions written as the gain and loss of hydrogen. The first experiment is a vibrant color variation using a synthetic dye of indigo carmine. The second…

The chemical experiment in this study is specifically created for undergraduate students studying energy and the environment. The target of the experiment is for students to comprehend the deactivation mechanism of the Ce/TiO[subscript 2] catalyst by oxides of phosphorus through practical experiments and enhance their knowledge of environmental…

We describe a three-day advanced organic laboratory experience that includes the solid-phase synthesis of an unknown three amino acid polypeptide for junior/senior undergraduate chemistry majors. Students conduct a series of 1D and 2D NMR experiments (HSQC, HMBC, TOCSY) and analyze the data to identify the side chain residues of the peptide and…

Thin-layer chromatography, which involves the movement of dyes along a silica-coated plate, is used to observe the progress of chemical reactions and to separate mixtures. We took advantage of this phenomenon to devise a method for generating patterns in the shape of numbers with dots (dot matrix). We prepared the azo dyes necessary for generating…