We present a simple smartphone-based protocol for the estimation of the critical micelle concentration (CMC) of surfactants. The protocol is based on contact angle measurements from the smartphone-captured images of differently concentrated surfactant solution droplets mounted over a naturally existing or chemically synthesized superhydrophobic…

A laboratory experiment was designed to introduce the practical application of biocatalysis in Bachelor and Master courses in biotechnology and medicinal chemistry, respectively. To this aim, the lipase from "Candida rugosa" was characterized (protein concentration and activity), immobilized on a carrier (by hydrophobic adsorption), and…

Contribution: This article proposes a low-cost and mobile device-based learning support system for the stepper motor, which provides Web-based remote laboratory. This system allows young engineers to learn about rotational principles, control methods, and programming in stepper motors. Background: Familiarity with electrical machinery, such as…

The reaction between hydrochloric acid and calcium carbonate to produce carbon dioxide gas is a popular and engaging experiment to illustrate chemical reactions that result in the production of gases. It also provides a useful model for teaching concepts related to the effects of concentration on reaction rates. Although a prepared hydrochloric…

This article describes low-cost well plates that can be used as alternative kits for microscale experiments. Although ordinary well plates are useful and convenient for microscale experiments, they are not cheap. We have developed well plates composed of plastic bottle caps with approximately 3cm diameter and cardboard containers. Plastic bottle…

Descriptive statistics involves summarizing and organizing data so that they can be easily understood. Even though these are basic and simple concepts, many applied science students have misconceptions about their use in applied experiments in the laboratory. Students usually receive limited or no training in how to understand the meaning of the…

A one-pot multicomponent synthesis of unsymmetrical indole-substituted methane derivative based on two consecutive reactions of p-methylbenzaldehyde with N-methylindole and 5,5-dimethyl-1,3-cyclohexanedione is described as an experiment that was carried out by second-year undergraduate chemistry students individually in a laboratory classroom. The…

S[subscript N]2 reactions are of fundamental importance in introductory organic chemistry courses, and a number of experiments suitable for the first-semester undergraduate organic lab have been previously reported. Most of these experiments have used alkyl halides as electrophiles, but alkyl halides are often less than ideal for reasons of…

Learning in chemistry laboratories has long been challenging due to the complex nature of the learning environment and tasks that students engage with. Therefore, it is important to develop useful tools for prelab and follow-up activities besides the hands-on lab time for better management of the learners' cognitive load. In this paper, we…

A [beta]-lactam, the core structure unit of clinically important antibiotics such as penicillin and cephalosporin, is one of the most commonly encountered four-membered heterocycles in organic chemistry and is widely used in medicine and biochemistry. The Kinugasa reaction, a copper­(I)-catalyzed cycloaddition of a terminal alkyne with a nitrone,…

A procedure to purify anthocyanin, a natural pigment, following a green approach by using macroporous resin and its encapsulation for the maintenance of its stability is described. This laboratory experiment, which describes the benefits of using resin for the purification, is a learning tool for students working in the field on nutraceuticals.…

We describe an experiment in which students use research-grade instrumentation to collect gas adsorption data in triplicate in a single 3 h laboratory period. The experiment reinforces the thermodynamic concepts taught in upper level physical chemistry courses and hands-on experience with instrumentation used in research laboratories. The speed of…

The area near the electrode surface is called the diffusion layer, and to understand electrochemistry, it is crucial that students have a knowledge of the phenomena occurring at the diffusion layer. Here, we present a demonstration and activity to visualize and analyze the expansion of a micrometer-sized diffusion layer. The electrode process…

Preparative chromatography is one of the most common and important purification techniques in organic chemistry and is employed in laboratories across the globe. In order to facilitate student proficiency with the method, a unique approach for the separation of estragole, ethyl cinnamate, and cinnamyl alcohol using microscale preparative flash…

The realities of accidents free situation in academic workshops and classrooms are anchored on strict adherence to laboratory safety rules and regulations, and normal classroom behaviour. The reality is less abided by Electrical/Electronic Technology students in classroom and workshops in the universities, causing accidents that lead to minor and…