An HPLC undergraduate experiment on the analysis of traditional Chinese medicine (TCM) has been developed. Two commonly used herbs ("glycyrrhizae radix" and "cinnamomi ramulus") are studied. Glycyrrhizin, cinnamic acid, and cinnamaldehyde are chosen as markers for the herbs. The dried herbs in their natural state and a TCM…

A detailed description of the synthesis of bis(1,2-dimethylimidazole)copper(I) hexafluorophosphate by using techniques in a glove box is presented. The results shows that the synthesis of the copper complex has a distinct color change indicating by-product oxidation by oxygen.

The first year undergraduates use a simple method to synthesize 5-nm CdS nanoparticles in a water-in-oil microemulsion. The quantum size effect, the relationship between colors, optical absorbance, band-gap energy and the CdS particles affected by the formation of micelles are observed.

The construction of an amperometric biosensor for glucose analysis is described demonstrating that the analysis is easy to perform and the biosensor gives good analytical performance. This experiment helped the students to acquire problem-solving and teamwork skills, allowing them to reach a high level of independent and critical thought.

The study describes the development of new biosensors based on metal nanoparticles because of its high surface area and large binding ability. The adopted procedure is extremely simple and versatile and can be used in various applications of electrochemistry.

An advanced undergraduate chemistry laboratory experiment to study the advantages and hazards of the coupling of NIR spectroscopy and chemometrics is described. The combination is commonly used for analysis and process control of various ingredients used in agriculture, petroleum and food products.

The Vitamin C Clock Reaction has now been adapted to serve as a student laboratory experiment in the education process of high-school and college-level general chemistry. Despite of imparting valuable knowledge, it also may be hazardous, as the tincture of iodine contains inflammable substances that may cause burning on prolonged exposure.

An experiment is designed where students will be using both gold and silver nanoparticles to study the enhancement factors of organic molecules adsorbed to the surface of the nanoparticles during or after synthesis by using surface-enhanced Raman spectroscopy (SERS). The experiment has helped students learn about the theory and experimental…

Experiments suited for the undergraduate instructional laboratory in which the heats of formation of several aliphatic and aromatic compounds are calculated, are described. The experiments could be used to introduce students to commercially available computational chemistry and its thermodynamics, while assess and compare the energy content of…

We suggest the creation of a Global Web Laboratory (we call it "GloLab") for scientific purposes and teaching experiments online. In this article, we discuss the main principles and problems of building such a global Internet-laboratory. An example of a current working laboratory for teaching magnetism experiments online is also discussed.

Described are several organometallic experiments for the homogeneous hydrogenation of alkenes that could be used in schools. Procedures and expected results are detailed. (RH)

The attempts of scientists to detect the existence of the medium of ether are traced. (DT)

A SCIENCE UNIT ON ORGANIZATION IS PRESENTED. THE OBSERVATION AND CATEGORIZATION OF LIVING THINGS ARE EMPHASIZED. STUDENTS ARE REQUIRED TO GATHER SPECIMENS OF PLANT AND ANIMAL LIFE AND TO LOOK FOR DIFFERENCES AND SIMILARITIES AMONG THEM. THIS COLLECTING AND GROSS SORTING OF SPECIMENS ARE ENCOURAGED THROUGH LABORATORY EXERCISES. DATA SHEETS ARE USED…