Crystal materials are an important pillar of advanced technology. Among them, the preparation of large-sized single crystal materials is of great importance for their practical application. Herein, we select the well-known nonlinear optical crystal KH[subscript 2]PO[subscript 4] and impressive deep-blue colored crystal CuSO[subscript…

A laboratory experiment was developed for the continuous flow preparation of an aminal derived from the condensation of furfural with morpholine. The experiment introduces the students to concepts of green chemistry, heterogeneous catalysis, and continuous flow. A cheap and easy setup allows the heterogeneous catalyst reactor to be built in class.…

Knowledge related to photochemistry has been gradually introduced as a part of chemistry courses at both undergraduate and postgraduate levels. However, due to their complex conceptual principles, limited class time, and tedious experimental setup and methodologies, students tend to encounter difficulties in understanding the concepts and…

Even though scientific communication and collaboration play critical roles in academic success, they often come in second to teaching laboratory fundamentals. COVID-19 associated capacity constraints forced our program to reexamine the traditional laboratory instruction paradigm by limiting physical attendance, as well as laboratory duration.…

Research-based pedagogy was implemented to enhance high school students' learning outcomes in basic organic chemistry. Flipped learning and structured peer work have been offered to grade 10 students(N = 12) during the course with appropriate classroom facilities, supervised by two facilitators. The preclass and in-class activities were designed…

In the modern and exciting world of particle physics, in which scientists talk of Higgs bosons and supersymmetry, it would be natural for someone to dismiss the common proton as a particle too pedestrian to be interesting. Yet in the centennial year of the announcement of its discovery, studies of the humble nucleus of the hydrogen atom continue…

Interaction forces between magnetic fields and current loops play a central role in the theory of magnetism. This work describes a reasonably simple and cheap experiment for demonstrating this issue: the force on a thin coil due to a nearby cylindrical magnet. The magnitude of the force as well as its attractive/repulsive character is comfortably…

In 2018, we celebrated the sesquicentennial birthday of Robert A. Millikan, a Nobel laureate in physics who worked among the greats such as Niels Bohr and Albert Einstein. His name, however, is perhaps not as widely known. He was born in 1868 in Morrison, Illinois, and moved with his family to the small town of Maquoketa, Iowa, at age nine. It was…

Additive colors are interesting to young students. In this paper, we show a convenient and straightforward method to demonstrate this phenomenon by projector. It produces defocus blur and reduces imaging quality for color mixing. We believe this demonstration experiment can be performed in most classrooms.

Physics and chemistry students learn several methods to determine the density of materials. While measuring the mass of materials is usually simple, volume measurements are more complex. For simple shapes the volume may be determined by measuring its geometry; for more complex shapes students often use Archimedes' principle. However, neither of…

Background/purpose: The current trend of training Chemistry teachers focuses on innovating pedagogical methods and developing students' holistic competencies, particularly their chemistry experimentation competencies (CEC). The CDIO (Conceive - Design - Implement - Operate) framework effectively combines theoretical knowledge with practice and…

This laboratory experiment employs an innovative approach to introduce undergraduates to liquid chromatography-tandem mass spectrometry (LC-MS/MS) by developing a method based on multiple reaction monitoring (MRM). During this qualitative investigation, students operated a triple quadrupole mass spectrometer in the MS scan and product ion scan…

An iridium(III)-mediated C-H functionalization sequence involving a concerted cyclometalation-deprotonation/migratory insertion pathway is reported for the undergraduate chemistry laboratory. The air- and water-stable iridacycle intermediates are readily isolated and characterized by NMR spectroscopy. Both steps of the experiment are performed at…

A high performance liquid chromatography (HPLC) experiment for the upper level analytical chemistry laboratory is described. The students consider the effect of mobile-phase composition and pH on the retention times of ionizable compounds in order to determine the acid dissociation constant, K[subscript a], of a phenolic acid. Results are analyzed…

In this paper, we propose a simple experimental apparatus that can measure the force variation over time to study the impulse-momentum theorem. In this proposal, a body attached to a rubber string falls freely from rest until it stretches and changes the linear momentum. During that process the force due to the tension on the rubber string is…