Undergraduate research experience is critical to success in postgraduate research settings. The recent movement away from "cookbook" style laboratories to course-based undergraduate research experiences (CUREs) in undergraduate laboratories has allowed universities to provide inclusive research experience while bypassing the limitations…

Mercury beating heart (MBH) is a well-known demonstration of redox processes. However, the development and application of the MBH system are significantly restricted due to its safety issues. Here, a direct current electric field-enabled gallium-based liquid metal heartbeat in a salt solution or alkaline solution is introduced as a demonstration…

A new undergraduate organic laboratory experiment has been developed for amide bond formation between biorenewable 2-furoic acid and either of two substituted piperazines to prepare medicinally relevant amide products using a procedure with industrial significance. The reactions proceeded smoothly under ambient conditions using the combination of…

In the past decade, C-H functionalization has been a very active topic of research in both academia and industry. When a H atom is replaced by an aryl (or heteroaryl) group, the transformation is termed "direct arylation". This approach to the formation of key (hetero)aryl-(hetero)aryl bonds is complementary to traditional methods, such…

The Joint Safety Team (JST) was conceived in 2012 by the Departments of Chemical Engineering and Materials Science and Chemistry at the University of Minnesota and the Dow Chemical Company as a model student-led safety organization. The JST initiative was aimed at improving academic safety through four core areas: compliance, awareness, resources,…

A multistep synthesis of quinolone antibiotic analogues was developed as a laboratory experiment for intermediate/advanced undergraduate students. Students can synthesize a range of "des"fluoroenoxacin analogues via a five-step sequence. The experiment includes a range of key practical laboratory techniques including thin-layer…

The experiment in charging and discharging of a capacitor through a resistor is fundamentally important for studying electronics. We have developed an alternative procedure to measure the voltage drops across capacitors as a function of time. The simple apparatus controlled by an Arduino Uno microcontroller board and LabVIEW™ interface was set up.…

A modified apparatus for measuring surface tension with the bubble-pressure method is proposed. Compared with a traditional instrument, this apparatus improved the accuracy of maximum pressure difference measurement and achieved the hydrostatic pressure correction. The apparatus was employed to determine the surface tension values of distilled…

The liquid nitrogen cloud demonstration is an effective, dramatic, large-scale demonstration to illustrate gas laws and cloud/fog (aerosol) formations for classes and large-scale outreach events. When performed at full scale, it is common to produce a cloud 20-30 feet in height. Its effect can be further enhanced by adding brightly colored…

We have investigated the motion of water flow through glass tubes of different shapes by calculating the value of the Reynolds number denoted as Re. We know that at a given flow rate the value of Re determines the type of flow being classified as laminar, transitional or tubulent. The dependence of Re in different configurations of glass tubes as…

A laboratory experiment that exposes students to fundamental concepts in kinetics and statistical thermodynamics to study systems of great current interest in nanotechnology by employing a foundational technique in physical chemistry is described. A modified commercial flash photolysis spectrometer was used to study photoinduced isomerization…

A laboratory experiment was developed for the continuous flow preparation of an aminal derived from the condensation of furfural with morpholine. The experiment introduces the students to concepts of green chemistry, heterogeneous catalysis, and continuous flow. A cheap and easy setup allows the heterogeneous catalyst reactor to be built in class.…

Here, students determine the total protein content in whey protein samples using the Lowry assay. Quantitative analysis was carried out using absorbance measured at 750 nm (standard method) and 96-well-plate digital images obtained using smartphones (proposed method). The proposed method was carried out using two smartphones (1 and 2). Smartphone…

In this paper, we discuss the theory of the operation and some practical considerations for the construction of an air ionization chamber, which can be used as a very simple detector of alpha particles. These detectors have several benefits compared to spinthariscopes and spark detectors. Classical experiments with ionization chamber detectors are…

As part of its STEM programming initiatives, Community Boating, Inc., the nation's oldest public sailing organization introduced an "Introduction to Microscopy" course merging principles of scientific investigation with analytical techniques using compound light microscopes. Boston's Charles River provided the environmental setting for…