The Griess assay is widely used by regulation agencies as an official method for nitrite quantification in water and food samples. In Brazil, the official method, which has been used to determine nitrite in food, was described by Instituto Adolfo Lutz (283/IV) in 1984. It uses 8 mL of reactants and provides 50 mL (reactants plus sample) of waste…

The practical two-step synthesis of 1-phenylthiourea is reported here as an undergraduate experiment for the organic synthesis laboratory. The reactions involved in 1-phenylthiourea preparation are very useful didactic examples to illustrate concepts relating to carbonyl substitution and addition, the effect of pH on solubility of organic…

A functionalized fiber (PAN[subscript ADMAP]F) was synthesized by immobilizing "N,N'"-dimethyl-"N"-(4-pyridinyl)-1,3-propanediamine (ADMAP, a DMAP analogue) onto the surface of polyacrylonitrile fibers (PANF). The structure and morphology of the functionalized fibers were characterized by Fourier transform infrared…

Surface chemistry impacts technology, advancing the development of new heterogeneous catalysts, semiconductor devices, and materials synthesis. Carbon surfaces are ubiquitous in various fields, and the surface reactivity can be altered by surface functionalization on the molecular scale, introducing functional groups, thus shifting their…

Anatomical sciences curricula have been under constant reform over the years, with many countries having to reduce course hours while trying to preserve laboratory time. In Mexico, schools have historically been autonomous and unregulated, and data regarding structure and methods are still lacking. A national survey was sent by the Mexican Society…

Electroscopes have been widely used in physics education for several reasons, such as their simplicity, sensitivity and visual appeal, showing macroscopic phenomena related to the microscopic world. Although they are capable of highly accurate measurements, the procedures involved in these measurements encounter some obstacles when performed with…

This paper describes an innovative, new, laboratory experiment conceived as a Senior Capstone Project by the student authors to provide experience with heat pipes for students in our junior-year Process Laboratory course at the University of Utah. Heat pipes can transport energy over long distances with minimal temperature gradients and no moving…

Gross anatomy courses utilize cadaver dissection to teach identification, topography, and spatial relationships of organs. The deconstructive nature of dissection, however, focuses students' attention on the "big picture", followed by a discovery of details. This approach may be useful for many, however some students may prefer to…

Contribution: An innovative teaching experience carried out at the University of Trento using team-based learning (TBL) in a large computer networks class. The impact of TBL on the students' learning and satisfaction was investigated. Background: Active learning pedagogies, including TBL, play an important role in enhancing higher-order cognitive…

Academic integrity is one of the significant issues facing assessments in higher education. While there are a plethora of papers addressing this problem in certain locales, very little research has been published regarding tertiary institutions in the Caribbean. This paper satisfies this paucity in the literature and present findings which will…

In his award-winning book, "Around the Texts of Writing Centers," R. Mark Hall (2017) asserts the importance of everyday writing center texts, claiming that these documents "both enact and forward writing center scholarship" (p. 3). It is Hall's position that such "everyday" documents are essential to understanding…

A comprehensive educational framework is provided by the Conceive-Design-Implement-Operate (CDIO) which is particularly relevant to engineering and applied sciences. This paper investigates the application of the CDIO approach in the field of chemistry pedagogy in Vietnam focusing on its adaptability to the current educational demands and its…

The undergraduates in the major of Environmental Science and Environmental Engineering frequently ignored the importance of identifying pollution sources for water environment monitoring and knew little about the techniques of identifying pollution sources. Thus, a laboratory experiment which focused on pollution sources identification in a water…

When laboratory accidents in schools, especially in recent years, are examined, it is remarkable that many of these events resulted from the incorrect implementation of laboratory safety. The most significant role in the administration of laboratory safety belongs to science teachers. During this process, the necessity of laboratory safety…

Hydrogen is a sustainable and climate-friendly storage for renewable energies and can directly be generated from sunlight, e.g., by photocatalytic water splitting. This article presents the photocatalytic hydrogen evolution using LED irradiation of an aqueous ZnS particle dispersion with Na[subscript 2]S and Na[subscript 2]SO[subscript 3] as…