A novel undergraduate analytical chemistry experiment involving the identification and quantification of linalool in essential oils was developed. The experiment uses the internal standard method with headspace solid phase microextraction (SPME) and gas chromatography--mass spectrometry (GC-MS). This method is applicable to any linalool-containing…

During the COVID-19 pandemic, many colleges switched to online or hybrid formats for both lecture and laboratory course delivery. While virtual experiments, that is, "dry lab" experiences, teach students chemical theory, it is essential for students in chemistry laboratories to participate in hands-on laboratory activities. These…

An integrated laboratory experiment was designed for introducing biochemistry students to basic static biochemistry to deepen their understanding on the properties and analysis of biomolecules such as total carbohydrates, lipid, protein, and protein-constituent amino acids. Food represents a very important source of biomolecules of technological…

In this study, we derived several formulas for the currents induced in a circular loop by a magnet connected to a spring-based simple harmonic oscillation system. In addition, we conducted an experiment for measuring the induced currents and compared the results with the theoretical prediction. It was confirmed that the prediction from the derived…

This study examined the effect of blended laboratory experiments on pre-service physics teachers' (PSPTs') attitudes toward physics laboratories. The research design was a quasi-experimental pre-test and post-test comparing groups. Participants were 63 2nd-year PSPTs' enrolled in a physics diploma program from three colleges of teacher education.…

Arduino is easy to use because it is a simple system. In addition, since Arduino has an open source code system, it is a system that is open to everyone's use, can be developed and can be easily implemented. Anyone who wants to use Arduino can buy and use the necessary parts for their application. It is a platform that can be very useful in the…

Optimization is a component critical to method development. Mathematical modeling of physical phenomena enables an efficient search for the parameters and conditions that optimize methods and systems. Here, optimization of methods in sonoelectrochemistry, electrochemical separations, electrochemical education, and assessment of diabetic status are…

An introductory normal phase column chromatography experiment is described and evaluated for second year undergraduate chemistry laboratory class. The experiment involves a nucleophilic substitution yielding a crude mixture of reactant and one product, both of which are brightly colored and contrasting, creating a clearly visual separation when…

This project introduces green chemistry to the undergraduate laboratory through two pedagogical techniques: undergraduate research and guided-inquiry. Through these two learning activities, an efficient synthetic procedure for the PRINS cyclization of citronellal into isopulegol, focused on minimizing negative environmental impact, was developed.…

A laboratory experiment was developed to introduce systems thinking and green chemistry concepts through the synthesis of the antidepressant and smoking cessation aid, bupropion hydrochloride. The traditional synthesis has several issues from a green chemistry perspective: it uses the toxic solvents N-methylpyrrolidinone (NMP) and dichloromethane…

Instrumentation plays a critical, ubiquitous role in modern chemistry. The undergraduate chemistry curriculum must therefore cultivate students' ability to investigate chemical phenomena via relevant instruments. The instructional laboratory serves as the primary context in which undergraduates learn about instrumentation, where use of instruments…

Catalysis and catalytic cycles are widely used in both research and industry. The addition of a catalysis experiment into the undergraduate laboratory curriculum is important and necessary training to expand student learning. Here, an experiment demonstrating iron-based tandem catalysis was developed and implemented in an organic chemistry course…

To remain globally competitive, education in the United States must focus on retaining students in science, technology, engineering, and mathematics (STEM). As laboratory courses have the potential to be powerful attractors or deterrents to a field, developing effective laboratory pedagogies is important to retain students in STEM. A course-based…

A drug discovery project has been successfully implemented in an advanced undergraduate organic chemistry laboratory. In the laboratory, a five-step synthetic sequence is used to prepare five analogues of 13-phenyl-1-tridecanol. These compounds are key precursors in the synthesis of 2-oxo-14-phenyltetradecanes. This class of compounds, isolated…

A straightforward procedure for the synthesis of (Ph[subscript 3]P)[subscript 3]CuCF[subscript 3], a robust, air-stable trifluoromethylating agent, is reported herein. This preparation can be completed in a single 3 h laboratory session and typically provides ample yields (~79--86%) and high purity (>90%). The target complex is characterized by…