Electrochemical impedance spectroscopy (EIS) is a rapid and powerful method for evaluating the pore structure of membranes. However, the application is limited due to the lack of appropriate training of engineers in electrochemistry and materials engineering. The introduction of laboratory practices can effectively improve the understanding of…

In recent years, the food industry has been undergoing major changes driven by new social and environmental demands. Nowadays, biodegradable packaging is perceived as the most feasible alternative for food packaging. Great efforts are being devoted to the development of new materials from agro-industrial wastes and byproducts that are opening new…

A laboratory experiment for the determination of the cross-linking density of silicone elastomers is described on the basis of swelling experiments and mechanical tests. In the experiment, the macroscopic swelling and mechanical behaviors of the elastomers were discussed as a function of the cross-linking density, which can be easily controlled by…

Flavor plays a crucial role and is the most important aspect of foods and beverages. [Beta]-Ionone is a common flavor compound with a characteristic violet-like odor. An undergraduate flavor compounds chemistry laboratory that provides preparation and characterization of the flavor compound inclusion complex between…

In this laboratory experiment, students apply a mass-based approach to determine the Henry's law constant for CO[subscript 2] using a small bottle of a diet carbonated beverage. The calculations are challenging; therefore, team-based learning is encouraged. Our students reported values of 0.033 ± 0.003 mol/(L[middle dot]atm) at room temperature…

This laboratory experiment introduces students to an important reaction in biomass valorization and allows them to gain a practical understanding of green chemistry. Acid-catalyzed dehydration reactions of fructose to 5-hydroxymethylfurfural and thus humins were performed both with and without aqueous solvent, along with two different catalysts…

This paper describes a new lab experiment where students explore the magnetic force on a permanent magnet placed inside a short solenoid. This lab is the fourth experiment performed in the second semester of the calculus-based introductory physics course at Washington University in St. Louis. The experiment is performed using a speaker (which…

An experiment was developed for a first year food chemistry laboratory course that demonstrates the influence of several aspects of polysacharide structure on the rate of amylase catalyzed hydrolysis. The experiment would be particularly well-suited to a first year chemistry course that was targeted at nonchemistry majors, such as health related…

Inorganic Chemistry teaches students the concept that modifications to ligand structures, especially the donor properties, can have a drastic impact on the reactivity and stability of the metal complexes. Experiments described here reinforce this concept through the investigation of two tetradentate ligands derived from…

In this article we describe the construction of a low-cost electronic device to adapt the widespread traditional approach of Analytical Chemistry teaching into laboratory experimentation based on the guided research model. To this aim we construct a portable electronic instrument based on the Arduino microcontroller and use it to develop various…

In general, undergraduate experimental physics laboratories do not usually have experiments designed to address rolling friction and to measure the value of the rolling friction coefficient. This work explores an experiment, which has the potential to arouse students' curiosity about rolling friction by addressing a counterintuitive aspect of the…

Nuclear magnetic resonance (NMR) spectroscopy has become a cornerstone tool for studying a variety of molecular features in advanced chemistry laboratories. In this experiment, students prepare a pyrrole-[beta]-amide via a one-pot, three-step synthesis and use NMR spectroscopy to confirm its molecular structure. In addition, variable temperature…

Green chemistry metrics and life-cycle analysis (LCA) were used to assess inefficiencies in two current organic chemistry experiments conducted in third-year organic chemistry to synthesize ("E")-stilbene from benzaldehyde. An alternative Wittig-based, greener, one-pot experiment using the same starting material was selected as a vehicle…

A research-style laboratory experiment for advanced undergraduate students is described, which includes the synthesis, characterization, and properties (porosity, stability, amphipathy) testing of the composite [Cu[subscript 2](BTC)[subscript 4/3](H[subscript 2]O)[subscript 2][subscript 6][HPW[subscript 12]O[subscript 40]·(C[subscript…

This work reports the first use of rubber latex waste as the hydrophobic reagent for a low-cost, simple, and rapid fabrication of a paper towel-based experimental device (PTED) with a circular design of 5 mm to demonstrate the factors affecting chemical equilibrium; this serves as a user-friendly means for a laboratory experiment. The illustration…