A safe, convenient, and environmentally benign laboratory experiment for the synthesis of biodiesel from six kinds of vegetable oils has been developed for the introductory organic chemistry laboratory. The experiment uses ultrasonic irradiation in the presence of a base catalyst at room temperature and atmospheric pressure. Because of safer and…

To understand critical problems associated with solid waste and its consequences for the environment, a laboratory experiment is presented on the synthesis of aluminum-based metal-organic framework (MOF) MIL-53(Al) from household waste (PET bottles and aluminum foil/can), for undergraduate students of chemistry. This work is designed to teach…

In the activity described in this communication, the authors present a simple experiment that can be implemented with moderate operational costs and that allows students to acquire the manipulative skills necessary for chromatographic analysis of a familiar fuel that still plays a fundamental role in providing energy for transport of passengers…

This laboratory experiment allows one to study the effect of temperature in the process of formation of hydrogen bound cyclic dimers of benzoic acid (BA). The implementation of the proposed methodology, which comprises the use of FTIR spectroscopy and quantum chemistry calculations, enables the obtaining of the thermodynamic parameters of the…

A laboratory experiment is detailed that entails the separation and derivatization of the artificial sweetener sucralose from a commercially available sweetener mixture. The experiment utilizes 1 g packets of a sucralose-based artificial sweetener and involves the separation of the synthetic sweetener from the more polar bulk additives by…

A laboratory experiment utilizing locally available Indian Gooseberry ("Phyllanthus emblica" Linn.) extract as a bioreagent to determine iron(III) is described with the goal of providing students with hands-on experience in spectrophotometry and green chemistry. Spectrophotometry was used to measure the concentration of the complex…

A laboratory experiment introducing the concept of chemical bioconjugation of proteins to undergraduate students in a therapeutically relevant context was developed. Initially, students installed an aldehyde functionality into a protein via the oxidation of the N-terminal threonine residue of the cholera toxin subunit B (CTB) protein, which was…

This paper reports an innovative, hybrid teaching model for a junior level lab course. This model leverages in-person lab operation by adding a student-led online learning mode. Both course outcomes and student outcomes were evaluated. Student feedback was collected, and its analysis showed both positive and negative impacts in this hybrid model.…

In this paper, we present data from two iterative teaching experiments involving students' constructions of four basic counting problems. The teaching experiments were designed to leverage the generalizing activities of relating and extending to provide students with opportunities to reflect on initial combinatorial activity when constructing…

Brewing science is an interdisciplinary course taught at many universities in both lecture- and lab-based modalities. The laboratory component of this class typically focuses on the brewing process from malted barley to beer. However, this ignores the malting process--an essential step in making beer, although one typically performed by maltsters…

With the enormous reliance on plastics in the world today, bisphenol A, an additive used in the synthesis of many plastics, such as polycarbonate, has been found almost everywhere in our environment including in soil, in natural waters, and inside organisms including humans. A multidisciplinary experiment is presented that involves using flatworms…

Dilute guarana´ ("Paullinia cupana") powder aqueous extract is a soft drink that contains three structurally related methylxanthines (MXs), caffeine (CF), theobromine (TB), and theophylline (TP); CF is present in a large excess. Literature data show that values of [lambda][subscript max] and [epsilon][subscript max] of these three MXs…

Frozen peas and carrots are commonly available in grocery stores in the United States. The carrots are cut into cubes roughly 8 mm on a side, while the peas are roughly spherical with a diameter of about 6 mm. They are prepared together in water that is brought to a boil. The peas and carrots, which are initially mixed together, separate as the…

White light refracted by a glass edge or a prism might be split into the colors of the rainbow but, when restricted by a suitable arrangement of edges, might also yield a sequence of colors complementary to the rainbow. We studied the creation of these color fields experimentally with a setup consisting of RGB light-emitting diodes that cover all…

Calculating the duration of a motion when the applied net force on the moving body changes with time is usually a challenging task. In most cases, the only example of the duration of a motion when the acceleration is not constant presented to introductory physics students worldwide is the example of harmonic motion. A discussion with respect to…