An integrated pair of experiments has been developed to introduce undergraduate students to the ways in which electrochemistry can complement conventional synthetic chemistry involving redox reactions. Students first use cyclic voltammetry and linear scan voltammetry to characterize and quantify the products of the reaction between…

A laboratory experiment is described in which students determine the concentration and speciation of iron in beer samples using cloud point extraction and absorbance spectroscopy. The basis of determination is the complexation between iron and 2-(5-bromo-2- pyridylazo)-5-diethylaminophenol (5-Br-PADAP) as a colorimetric reagent in an aqueous…

The convenient synthesis of dihydroberberine by the reduction of berberine is described as an experiment for an upper-division undergraduate organic chemistry laboratory course. Students obtained up to 74% yield of the desired pure product without the use of chromatographic techniques. The antimicrobial activities of both compounds against…

The article presents the results of four series of experimental studies of irradiation efficiency of Moskovskii Parnikovyi leaf lettuce with general and special-purpose LED lamps (phyto-lamps) under various irradiation modes. The studies were conducted with an automated experimental irradiation device. The influence of the spectral compositions of…

The anomalous thermal expansion of water in the 0 °C-4 °C range is extremely important to life on Earth, but it is normally not presented experimentally in educational settings. This paper presents a simple experiment to explore the anomalous thermal expansion of water in the 0 °C-4 °C range and the heat exchange processes in natural bodies of…

An experiment to match five white solids with ascorbic acid, citric acid, potassium hydroxide, sodium chloride, and urea is reported here. This 4 h experiment is an integrated practice of two experimental techniques, calorimetry and titration. Students conduct an extensive literature search on the properties of the five compounds and plan the…

Recently, small computer fans have been demonstrated to be an effective method for teaching simple resistive circuits both qualitatively and quantitatively. The current through the fans is related to the rotational speed of the fans and allows multiple senses to be engaged (touch, sight, and hearing). Methods for learning simple circuits in an…

Is a suction cup at the bottom of a bathtub subject to an upward force from the surrounding water, even if there is no water under it? A student question, posted in a teacher facebook group on a Monday morning, led to a discussion involving 21 comments with 225 replies offered by 16 teachers during the next few days, including several simple…

A simple experiment is described to verify the current dependence of Ampère's law for a long straight current-carrying conductor. A narrow and long rectangular multi-loop design is used to increase the strength of the magnetic field in between the long sides. As expected, the magnetic field is found to be linearly proportional to the electric…

The study of buoyancy is common in physics classrooms. In the last 20 years, several educators have described, theoretically and experimentally, buoyant forces and Archimedes' principle, both in "The Physics Teacher" and elsewhere. However, as far as I know, no one has reported on the pedagogical implications and experimental results of…

We have added two improvements to a self-luminous LED stroboscope (a flashing point-like projectile developed for introductory mechanics): downsizing by replacing heavy and risky batteries with a compact and safe capacitor of several Farads (a so-called Super-C) and wireless control via ordinary IR (infrared) communications. Consequently, the…

An alternative way of introducing magnetism at all levels of education is proposed. It is stressed that magnetism can be introduced through the interaction between current-carrying conductors giving the students, at the same time, the possibility to measure the magnetic permeability [mu][subscript o]. Focusing on currents instead of permanent…

Protein PEGylation refers to the covalent binding of polyethylene glycol (PEG) moieties to a protein and has been increasingly applied, mainly in the biopharmaceutical industry. This technique may increase bioavailability and stability by decreasing immunogenicity and proteolytic attack. Given the industrial interest and the relevance of this…

Chronic stress typically leads to deficits in fear extinction when tested soon after chronic stress ends. Given the importance of extinction in updating fear memories, the current study examined whether fear extinction was impaired in rats that were chronically stressed and then given a break from the end of chronic stress to the start of fear…

A laboratory class was developed and evaluated to illustrate the synthesis of metal nanoclusters (NCs) and to explain their photoluminescence properties for the case of silver. The described experiment employs a synthetic protocol that consists of two sequential phases in a single reaction pot: the reduction of silver ions into plasmonic silver…