Biochemistry is about structure and function, but it is also about data and this is where computers come in. From my time as a graduate student and post doc, whenever I encountered data I thought, "I can work this up by hand, but I think a computer could do a better job." Since that time, I have been working at the interface of…

Chemistry in water is an emerging field that fulfills the fifth principle of green chemistry: replacing toxic organic solvents with their benign counterparts. Although some pharmaceutical industries have developed and adopted chemistry in water, its implementation in teaching laboratories is still limited. Therefore, we have designed an experiment…

This work presents a homemade multirole 3D-printed modular spectrometer(MPMS), which can be easily assembled like bricks and expanded with several modules to measure different types of spectra, such as UV-vis absorption, fluorescence emission, flame emission/absorption, glow discharge, and even Raman spectra. The spectrometer is designed to be…

Microplastics have been detected in most ecosystems around the world. They affect the environment and organisms in it, including humans and possibly their health. Hence, the analysis of microplastic occurrence in the environment is highly relevant. However, there are only a few practical and easy-to-implement methods published for school use, and…

We report here a successful adaptation of lab videos used during remote instruction to a kinetics experiment reported in this Journal in 2007. In the in-person lab, students now record their rate data on their cell phone cameras and then collect their data from the videos for their postlab reports; previously, they acquired the data in real time…

A two-component undergraduate laboratory experience has been developed by students in a senior level capstone course. The first component is a 3 h laboratory experience dedicated to the rapid synthesis of a metal-organic framework (MOF-808) in aqueous solution using readily available reagents and equipment. During the second component, MOF-808 was…

A cooperative-learning jigsaw-style activity was developed to create opportunities for introductory organic chemistry students to discuss and decipher [superscript 1]H NMR spectra. Students cooperatively interpreted spectra that contained both pure and mixed solvents, building consensus through explanation and argumentation on what each spectrum…

The laboratory is a complex environment where the three levels of the chemistry triplet coincide. As the laboratory environment places a large demand on the working memory of students, cognitive load theory can address overload which causes barriers to learning. Breaking down barriers requires iterative phases of analysis/exploration,…

A research-style laboratory experiment composed of the synthesis of MOF-74 materials, related structural characterization, and the cutting-edge application of electrocatalytic oxygen evolution reaction (OER) has been designed toward advanced undergraduates at East China University of Technology (ECUT). The desired monometallic MOF-74 (Ni-MOF-74…

A modern cybernetic potentiostat plays a significant role in realizing various electrochemical measurements. This technology report describes a general-purpose, scalable, handheld (10 cm[superscript 2]), yet affordable hardware-software framework for a potentiostat, galvanostat, and electrochemical impedance spectrometer with high capabilities:(1)…

Fractional distillation is part of the essential experimental techniques taught to first-year chemistry students, especially during practical organic chemistry work. The characterization of the distillate generally involves measuring the boiling temperature, the refractive index, or the infrared spectrum. In this paper, an unknown mixture composed…

Photo-oxidation is one of the main causes of oxidative deterioration in food. Understanding of the mechanisms of photo-oxidation is essential for food science students when pursuing careers in food safety and quality assurance. However, few food chemistry laboratories emphasize photo-oxidation. Thus, we develop a laboratory activity that trains…

We here propose a simple and fast hands-on activity requiring limited equipment, to introduce students of various levels (bachelor's or high school) and backgrounds (from science to arts) to the chemistry of color. The different colors of stained glass are replicated through the deposition, on ordinary glass slides, of silica coatings colored by…

The provision of feedback with complex information beyond the correct answer, that is, elaborated feedback, can powerfully shape learning outcomes such as transfer, that is, the ability to extend what has been learned in one context to new contexts. However, an understanding of neurocognitive processes of elaborated feedback during…

As an alternative to the traditional metallocene laboratory targets, students synthesize Cp[subscript 2]TiCl[subscript 2], bis([eta][superscript 5]-cyclopentadienyl)dichloridotitanium(IV), from the mildly moisture-sensitive cis-TiCl[subscript 4](thf)[subscript 2]. Air-free handling techniques are emphasized, but the (mostly) air-stable,…