The helium-plasma (HePI) ionization mass spectrometry method was used to track the formation of reaction products and consumption of reactants by continually monitoring the vapors in the reaction headspace in real time. Two examples of the application procedure are presented here: a nucleophilic acyl substitution reaction and a 1,4-nucleophilic…

An introductory experimental course to teach and assess basic organic synthesis and identification skills has been designed. The first work of this course, which is based on the well-known hydrazone formation reaction of benzaldehydes with Brady's reagent, is presented. The designed experiment has many advantages and perfectly matches the goal of…

Photochemical reactions are the reactions that are induced by light. Many of these reactions are found in natural processes, including photosynthesis and the formation and decomposition of ozone in the atmosphere. Classroom demonstrations are effective in enhancing students' learning and retention. Herein, we have developed a simple demonstration…

The addition of research-focused experiences to undergraduate chemistry laboratory courses has been shown to bolster student learning, enhance student retention in STEM, and improve student self-identity as scientists. In the area of synthetic organic chemistry, the preparation of libraries of compounds with novel optical and electronic properties…

When structure-property relationships are discussed in inorganic chemistry and materials science, the common perception is that materials with the same composition and atomic arrangement have the same properties. In this laboratory experiment, we show that "processing"--the exact conditions under which materials are made--can in fact…

The COVID-19 pandemic was an unprecedented event that, out of necessity, drastically changed the way undergraduate chemistry courses were taught. With the cancellation of in-person classes, laboratory experiences were delayed and/or moved to the virtual space, the latter keeping the general framework of the laboratory experiment but removing the…

This article describes an exercise for a physical laboratory experiment designed to enable physical geography students to practice transferable quantitative skills through inquiry-based learning. The exercise is a deliberately simplified physical model of storm-driven coastal overwash typical of low-lying coastal barrier systems. The experiment…

A renewed experimental procedure for the unknown carbonyl experiment has been developed using hydrazone synthesis, thin layer chromatography (TLC) analysis, and melting point determination to differentiate between structurally similar ketones and aldehydes in undergraduate organic chemistry practical courses. Benzaldehyde, p-tolualdehyde,…

Clathrate hydrates are attractive materials for education because they form from water and familiar compounds, such as carbon dioxide, and are relevant to novel technologies. In this study, an attempt to propose a laboratory experiment was summarized, which used carbon dioxide clathrate hydrate as an educational material with carbon capture…

Aim/Purpose: The study seeks to utilize Augmented Reality (AR) in creating virtual laboratories for engineering education, focusing on enhancing teaching methodologies to facilitate student understanding of intricate and theoretical engineering principles while also assessing engineering students' acceptance of such laboratories. Background: AR, a…

Laboratories are considered to play a unique role in circuits teaching. Laboratories can be traditional, with physical components and desks, or virtual with graphical simulators. Applying these facilities in teaching, students can make experiments or measurements by exploring electric circuits' features. However, an intriguing research question is…

The literature on laboratory objectives in engineering education research is scattered and inconsistent. Systematic literature reviews identified the need for better understanding. This paper ranks the laboratory learning objectives across the cognitive, psychomotor and affective domains to improve scaffolding. It provides an opportunity for…

In today's world, remote-controlled robots are widely used across various industries due to their ability to enhance working efficiency in various applications. Learning about robot operation and human-computer interaction has emerged as a popular topic in recent times. Indeed, learning robotics can be challenging for many students as it requires…

In this two-session experiment for an organic chemistry lab, students prepare a macrocyclic host compound--namely, a pillar[5]arene--by means of a templated 1,4-dimethoxybenzene/formaldehyde cyclo-oligomerization (session 1), and then, they explore its molecular recognition properties toward the 1,8-diaminooctane guest with the aid of [superscript…

Discussion-based outcomes of organic chemistry laboratory experiments form a powerful tool to create a learning environment, facilitate teamwork, and build scientific skills and analytical ability for undergraduate science students. A Knoevenagel-type condensation reaction was selected to demonstrate these results by taking phenylacetonitrile and…