Nuclear magnetic resonance (NMR) spectroscopy has become a cornerstone tool for studying a variety of molecular features in advanced chemistry laboratories. In this experiment, students prepare a pyrrole-[beta]-amide via a one-pot, three-step synthesis and use NMR spectroscopy to confirm its molecular structure. In addition, variable temperature…

Green chemistry metrics and life-cycle analysis (LCA) were used to assess inefficiencies in two current organic chemistry experiments conducted in third-year organic chemistry to synthesize ("E")-stilbene from benzaldehyde. An alternative Wittig-based, greener, one-pot experiment using the same starting material was selected as a vehicle…

Scaffolded inverse blended learning (SIBL) enables self-paced, individualized learning by incorporating different levels of learning activities. The SIBL approach is described for an online general chemistry course enhanced with face-to-face interactions for first-year students in an institute of higher learning. It can be easily modified and…

Whether it is prolonged strike action, a protest movement, or a global viral outbreak, the disruptions triggered in higher education are profound. In a STEM subject, laboratory classes are vital to teaching and learning. Chemistry educators had to transport laboratory skills-based teaching and assessment of courses to the virtual world at short…

While the suspension of face-to-face instruction disrupted laboratory components of most chemistry-based classes at the college level, it was notably disruptive to upper-level chemistry courses based solely on laboratory experiences. This communication describes the logistical and pedagogical efforts made in an integrated, upper-level,…

The COVID-19 pandemic has caused the loss of many lives and transformed the global educational system. This has resulted in a rapid transition from face-to-face classroom meetings to online education delivery. Online education provides another opportunity to engage students during crises, such as pandemics. However, during the transition to online…

Because of COVID-19 precautions, instructors worldwide were required to introduce a variety of virtual instruction modes to complete the Spring 2020 semester. Herein we describe parallel efforts in contextualized chemistry courses at two institutions--Carthage College and Central Michigan University. These courses are primarily designed for…

This work reports the first use of rubber latex waste as the hydrophobic reagent for a low-cost, simple, and rapid fabrication of a paper towel-based experimental device (PTED) with a circular design of 5 mm to demonstrate the factors affecting chemical equilibrium; this serves as a user-friendly means for a laboratory experiment. The illustration…

After a grueling grading campaign, a chemist asked a writing and rhetoric specialist for help improving formal reports in the introductory organic chemistry lab. Together, we realized that the very best student reports employ many persuasive moves in the combined results and discussion subsection, whereas weaker papers omit the persuasive…

The topic of atomic spectra is part of university and secondary school curricula around the world. Relatively little research, however, has been done on the learning and teaching of this subject, despite the fact that it forms a foundation for advanced study in quantum mechanics, astronomy, and astrophysics. A systematic investigation into student…

Pharmaceutical analysis, as the core curriculum of chemistry, chemical engineering, and pharmaceutical engineering, contains broad and in-depth knowledge that leads to massive learning and teaching loads. There are more than 100 analytical methods of medicines in this course. As such, this subject is a big challenge for both students and…

This paper examines the current state of the implementation of green chemistry into organic chemistry textbooks. Content analysis of the 15 most used organic chemistry textbooks revealed that only 10 of them had any mention of green chemistry. In textbooks that contained mentions of green chemistry, it was mentioned on less than 1% of pages. Green…

Fast, reliable, well-resolved latent fingerprints can be planted by applying a thin coating of a 50:50 mixture of hand lotion and food-grade protein powder. Fingerprints can be revealed with iodine fuming or ninhydrin staining. This low-cost alternative to commercial latent print pads can be used in a variety of classroom or public settings where…

Introducing chemical equilibrium concepts in undergraduate general chemistry promotes improved understanding of chemical reactions. We have developed an engaging laboratory experiment exploring the equilibrium of cobalt complexation in alcohols using UV-vis spectroscopy and successfully implemented in a large general chemistry class of 378…

A contemporary undergraduate laboratory experiment incorporating parallel microscale experimentation was developed for the well-defined palladium catalyzed Suzuki-Miyaura cross coupling of 4-fluorophenylboronic acid with both 4-chloro- and 4-bromoanisole using 11 diverse phosphine ligands and one ligandless control. This laboratory introduces…