Electrophilic aromatic substitution reactions are common in the organic chemistry laboratory. These reactions, while ubiquitous, use corrosive reagents and halogenated or hydrophobic solvents that produce expensive and hazardous waste streams. The carboxylation of phenols (Kolbe-Schmitt reaction), although aqueous, typically involves conditions…

The COVID-19 pandemic and its related restrictions forced the reorganization of learning methodology and gave a central role to remote learning. Laboratory experiments are the most affected activity, and several alternatives were described. This work proposes to create calculation tools by simply programming in Visual Basic of Excel to emulate the…

Assessments that are open-ended and student-centered may be used to encourage formation of networks between prerequisite material and new course content thereby promoting meaningful learning. Creative Exercises (CEs) are assessments that allow multiple correct answers and do not penalize for incorrect statements thereby inspiring creativity. CEs…

Electrochemistry is taught in most undergraduate chemistry programs. Although this topic is important for students due to its broad interest in industry (energy, diagnostics, car industry, etc.), they often find it difficult, because it is based on a combination of various physical concepts such as electric fields, interfacial processes or charge…

The construction and characterization of a glucose biosensor has been implemented in an instrumental chemical analysis course to provide students experience with chemical sensing, electroanalytical methods, and flow injection analysis (FIA). The glucose biosensor was assembled on a glassy carbon electrode by depositing a layer of Prussian blue…

An advanced research discovery laboratory course in inorganic chemistry has been developed to engage undergraduate students in authentic research experiences directly related to concepts and theory taught in the lecture portion of the course. The 12-week laboratory involves an initial 4 weeks of training experiments on inorganic/organometallic…

An approach to online laboratory exercises for analytical chemistry students with demonstrated practical exercises through the use of remote-controlled gas chromatography (GC) instrumentation is discussed. The approach allows for a practical-based learning activity to be carried out by students who are unable to attend in-person laboratory…

Performing HPLC-based experiments in the undergraduate practical classroom is difficult because of the time required to perform an analysis. This limits the type of practical to one that undertakes a simple quantitative analysis. However, with the use of sophisticated simulators, such as the one employed in this exercise, more complex experiments…

Here, we describe strategies for integrating transferrable professional development (PD) skills into research learning environments for marginalized undergraduate students. The undergraduate research experience evolved to include the competencies students need to be successful and to gain a sense of belonging in the chemistry community they are…

Applications of machine learning in chemistry are many and varied, from prediction of structure-property relationships, to modeling of potential energy surfaces for large scale atomistic simulations. We describe a generalized approach for the application of machine learning to the classification of spectra which can be used as the basis for a wide…

Laboratory skills assignments were developed as a novel approach to providing students with the opportunity to engage in hands-on laboratory skills development outside of the lab during the COVID-19 pandemic. Initially, the assignments were implemented within a second-year forensic chemistry course of 48 students and redesigned and modified to be…

Experiments serve different purposes in chemistry education ranging from illustrating a certain subject matter to providing data for school-based research projects. When students use these experiments to collect data and draw conclusions, it is important that these experiments are valid. In this study, a new experiment for the determination of the…

Common over-the-counter medicines can be an exciting entry point for introducing students to the interesting chemistries that they encounter in their daily lives. In this inquiry-based activity, students are tasked with using a list of given supplies and information about four medications (Aspirin, Tums, Pepto-Bismol, and Tylenol) to design three…

In this paper, a problem set activity focused on understanding and applying unsupervised and supervised chemometric methods for the analysis of biodiesel-diesel blended fuels is described. This problem set was utilized in two upper-level analytical elective courses aimed for junior and senior level students. The data set consists of peak areas…

It is crucial nowadays to predict in a fast and simple manner physical-chemical behaviors like, the size-dependent optical properties of gold nanospheres (Au NSs). The idea behind this experiment is trying to replace (as much as possible) robust and expensive microscopy techniques with UV-vis spectrophotometry and friendly simulations. Students…