Biodiesel is an important biomass, largely employed in the transport sector and produced from vegetable oils. Additionally, waste cooking oils may be reused to produce biodiesel fuel, minimizing environmental pollution. A laboratory experiment that affords a widespread way to discuss degradation concepts and tools for used vegetable oil…

For conducting laboratory experiments on Fresnel diffraction, the use of a simple point light source from an LED and the application of a modern smartphone for photographing the diffraction patterns are proposed. The developed devices allow the experiments to be carried out under normal laboratory lighting.

When injecting dye into a vortex, one finds that the dye remains captured around the vortex core over minutes, despite the fact that the vortex (and the dyed region) is strongly time-dependent. According to a recent theory, three-dimensional time-dependent vortices should be defined as rotating, material-holding regions of the fluid. Vortices…

Carbohydrates are an essential group of molecules to the organic chemistry classroom providing molecular relevance to a common ingredient in chemical biology. While the meticulous elucidation of the carbohydrate structures by Fischer and others is an engaging topic in the lecture, there are few laboratory experiments that can emulate carbohydrate…

This communication describes a method to detect aluminum in gastric drugs by the naked eye using a microfluidic paper-based analytical device ([mu]PAD). Aluminum ions react with chrome azurol S (CAS) and cetyltrimethylammonium bromide (CTAB) to form a colored complex, which generates a colored band on the [mu]PAD. A printed ruler can be used to…

A continuous flow photopinacol coupling of benzophenone has been developed and implemented in the undergraduate laboratory. This photoreduction was accomplished using 2-propanol as an H atom donor and cosolvent in the reaction. The simple and inexpensive UV light source and flow reactor design (less than $350/photochemical flow system) provide an…

Williamson ether experiments are commonly performed by students in undergraduate organic chemistry instructional laboratory courses. In this multioutcome experiment, students were provided 4-bromophenol and one of three alkyl halides: 1-bromopentane, 1-bromobutane, or 1-bromo-3-methylbutane. The alkyl halides served as the unknown component of the…

A laboratory experiment characterized by a whole-class data-pooling approach to generate a data set that can be used to test a model of the influence of ionic strength on electrolyte solubility is described and discussed. The design of the experiment makes efficient use of the laboratory period and releases time for instructional and dialogic…

How well does the undergraduate organic chemistry laboratory curriculum prepare students for academic research, or for a bench job in industry? Running experiments that are more representative of research chemistry has the potential to better equip students for working in a research laboratory, while at the same time giving them insight into a…

These days, smartphones are popular commodities among students in high school and college. Students carry their devices all the time, so why not use such a popular electronic device to measure physical quantities such as "g" in physics labs? In this work, we report a "multiple tasking" method, a measurement technique that we…

An undergraduate organic chemistry experiment has been developed that features asymmetric synthesis of an enantioenriched secondary alcohol, followed by determination of its absolute configuration using the competing enantioselective conversion (CEC) method. Students are given a ketone and an unknown enantiomer of CBS (Corey-Bakshi-Shibata)…

Enzymes are widely applied in different industries, like pharmaceutical, food, biofuel, and waste valorization. However, the enzyme operating conditions are very limited. So, in most industrial processes, enzymes are not efficient, due to the use of harsh conditions, like organic solvents, extreme pH, and temperature. Immobilization arises as a…

This study is the result of a quantitative analysis of the previous paper reporting on four cases in which an LED is turned on by charge transfer occurring during the electrostatic induction process in a conductor connected to the LED. We were able to measure the charge transfer by using charge sensors and analyze experimental results by applying…

With the advancements in broad-spectrum sunscreens and the recent bans on benzene-based sunscreens due to their environmental toxicity, there has been a push toward broad-spectrum sunscreens containing in organic active ingredients. In this study, a procedure was developed to analyze the particle size and size distribution of inorganic active…

This paper uses evidence-centered assessment design (ECD) to structure and analyze a laboratory activity where students collect and represent titration curve data to determine acid strength in terms of molarity and dissociation constant. Following principles of multidimensional learning, the activity prompts students to demonstrate knowledge of…