An undergraduate organic chemistry laboratory experiment that provides an introduction to the concepts and practices of photoredox catalysis is reported. While undergraduate-level photochemistry experiments typically place emphasis on analytical properties of catalysts rather than synthetic applications, this experiment showcases the power and…

Polymer chemistry is an integral part of art conservation graduate training programs. The list of materials used by artists and artisans and by conservators is vast, with the majority being polymeric in nature. Conservators use an array of polymers as coatings, adhesives, fills, supports, and structures. Aside from the chemistry of these…

The study of buoyancy becomes very interesting when we measure the apparent weight of the body and the liquid vessel weight. In this paper, we propose an experimental apparatus that measures both the forces mentioned before as a function of the depth that a cylinder is sunk into the water. It is done using two load cells connected to an Arduino.…

Surface modification has been considered as a fundamental item in upper-division undergraduate and master courses. Thus, the development of experiments regarding processes and characterization of surface-modification phenomena is highly desired. In this article, we propose an electrochemical and computational study of widely used…

An interdisciplinary laboratory experiment was designed and carried out on the basis of the photo/electrochromism of N,N'-bis(cysteine)pyromellitic diimide (BCPD), suitable for organic chemistry laboratory I and physical chemistry laboratory II students. In the organic chemistry laboratory, students synthesized BCPD and studied its…

An integrated pair of experiments has been developed to introduce undergraduate students to the ways in which electrochemistry can complement conventional synthetic chemistry involving redox reactions. Students first use cyclic voltammetry and linear scan voltammetry to characterize and quantify the products of the reaction between…

A laboratory experiment is described in which students determine the concentration and speciation of iron in beer samples using cloud point extraction and absorbance spectroscopy. The basis of determination is the complexation between iron and 2-(5-bromo-2- pyridylazo)-5-diethylaminophenol (5-Br-PADAP) as a colorimetric reagent in an aqueous…

The convenient synthesis of dihydroberberine by the reduction of berberine is described as an experiment for an upper-division undergraduate organic chemistry laboratory course. Students obtained up to 74% yield of the desired pure product without the use of chromatographic techniques. The antimicrobial activities of both compounds against…

Lab-based learning is an essential part of any undergraduate chemistry curriculum as it incorporates necessary and required hands-on experiential learning. However, in response to the COVID-19 pandemic, many students are learning from home, rendering laboratory instruction a particular challenge. Options for educators include third party virtual…

One of the most general aims of universities is to respond to the requirements of society. Health and safety are the most important aspects of professional work and play an important role in universities, as there, future professionals are trained for their future professional life. Scientific and technical degrees require adaptation to this…

The Griess assay is widely used by regulation agencies as an official method for nitrite quantification in water and food samples. In Brazil, the official method, which has been used to determine nitrite in food, was described by Instituto Adolfo Lutz (283/IV) in 1984. It uses 8 mL of reactants and provides 50 mL (reactants plus sample) of waste…

Lampworking is a valuable skill for students in Chemistry and others in science, technology, engineering, and math (STEM) related fields. The activity described here provides instructors the resources to both learn and teach the fundamentals of lampworking. Soft glass, which can be shaped and fused with a Bunsen burner, is used to improve the…

This work shows the redesign of an elemental experience based on the Helmholtz resonator using 3D printing. A Helmholtz resonator is based on a volume and at least one opening that can include a tube or not. The air column inside the tube can be considered the mass of the system, whereas the volume represents the system's stiffness. Due to these…

The framework of ecosystem services (ES) and disservices (ED) has increasingly been used in various science, technology, engineering, and mathematics (STEM) disciplines, including soil science. The objectives of this study were to use ES/ED concepts to extend and test an existing lecture and laboratory exercise on soil organic carbon (SOC) in an…

Laboratory practical sessions are critical to scientific training in biology but usually fail to promote logical and hypothesis-driven reasoning and rely heavily on the teacher's instructions. This paper describes a 2-day laboratory practicum in which students prepare and analyze larval cuticle preparations of "Drosophila" segmentation…