A simple experiment about thermal effects in chemical reactors is described, which can be used to illustrate chemical reactor models, the determination and validation of their parameters, and some simple principles of heat transfer and sensor dynamics. It is based in the exothermic reaction between aqueous solutions of sodium thiosulfate and…

The generally accepted method to determine iron content in food is by acid digestion or dry ashing and subsequent flame atomic absorption spectrometry or inductively coupled plasma atomic emission spectrometry. We have developed an experiment that chemically extracts the iron from an egg yolk and quantifies it using UV-vis absorption…

Diapocynin (5,5'-dehydrodiacetovanillone) was synthesized by oxidative coupling of apocynin (acetovanillone, or 4-hydroxy-3-methoxyacetophenone). Diapocynin is a metabolite of apocynin, which has anti-inflammatory and anti-oxidative properties. The oxidizing agent was an in situ generated sulfate radical, produced by adding iron(II) sulfate and…

In this article I review one of the most significant accomplishments of Frank H. Westheimer, one of the most respected chemists of the 20th century. This accomplishment was a series of stereospecific enzymatic oxidation and reduction experiments that led chemists to recognize what we now call the enantiotopic and diastereotopic relationships of…

Plant-derived phenolic compounds such as those found in red wine, tea, and certain fruit juices may protect against cardiovascular disease by detoxifying (scavenging) superoxide and other unstable reactive oxygen species. We present a laboratory exercise that can be used to assess the superoxide-scavenging capacity of beverages. Among the…

An experiment and a demonstration concerning transport by magnetic levitation (Maglev) are described. The lift, drag and radial forces on a magnet placed over a rotating conducting disc are measured versus the rotation frequency. The experiment relates to important topics of electromagnetism and could be a useful addition to the undergraduate…

In this paper, we report the development of an automated system for energy bandgap and resistivity measurement of a semiconductor sample using Four-Probe method for use in the undergraduate laboratory of Physics and Electronics students. The automated data acquisition and analysis system has been developed using National Instruments USB-6008 DAQ…

Preservice elementary education students often do not have a good feel for the process of science. Many may be acquainted with the steps of the scientific method but have never been through the scientific process. An exercise was designed using temperature-logging iButtons (Thermochrons) to improve knowledge of and familiarity with the process of…

To determine the carbonation degree of materials used in mineral carbonation experiments, a fast, simple, and sufficiently accurate method is required. For this purpose, a method based on the reaction between carbonates and hydrochloric acid was developed. It was noted that this method could also be used to teach undergraduate students some basic…

A simple, sensitive, and portable viscometer has been designed using an opto-mechanical mouse. The viscosity of a fluid is measured using the infrared light-emitting diodes and the optical diodes of an opto-mechanical mouse. These components are positioned near the top and bottom of a glass tube containing the fluid to be measured. The viscosity…

A series of online interactive teaching units have been developed that illustrate the use of experimentally measured three-dimensional (3D) structures to teach fundamental chemistry concepts. The units integrate a 500-structure subset of the Cambridge Structural Database specially chosen for their pedagogical value. The units span a number of key…

In this solar panels and alternative energy project, students were challenged to develop a researchable question about solar energy and electronics and devise a means of answering it. Students worked cooperatively, with specific roles for each member, conducting research, conducting experiments, analyzing results, and writing the final…

A basic setup for data acquisition and analysis from an oscillatory circuit is described, with focus on its application as either low-pass, high-pass, band-pass or band-reject frequency filter. A homemade board containing the "RLC" elements allows for the interchange of some of them, in particular, for the easy change of the "R" value, and this…

This paper discusses how the Carnot engine led to the formulation of the second law of thermodynamics and entropy. The operation of the engine is analysed both in terms of heat as the caloric fluid and heat as a form of energy. A keystone of Carnot's thinking was the absolute conservation of caloric. Although the Carnot analysis was partly…

We have used the recently developed method for rapid measurement of maximum density temperature to determine the rate at which hydrogen and deuterium isotope exchange takes place when a sample of heavy water is exposed to the atmosphere. We also provide a simple explanation for the observed linear rate of transition. (Contains 2 figures.)