We developed a single crystal X-ray crystallography experiment based on the crystal structure of sucrose (table sugar), and a more challenging experiment using Epsom salt. Both crystals are readily available in X-ray quality crystalline form. In these experiments, students mounted a crystal on a MiTeGen loop and analyzed it using a Rigaku XtaLAB…

Owing to the global spread of the coronavirus disease 2019 (COVID-19), education has shifted to distance online learning, whereas some face-to-face courses have been resumed with the improvement of the outbreak prevention and management situation, including a laboratory course for senior undergraduate students in chemical biology. Here, we present…

In the course of combining the Sustainable Development Goals (SDGs) with the science education curriculum, the relevance of the micro- and macroalgae in education is based on the biotechnological future-oriented significance and the ever-growing trend toward plant-based nutrition. So, the micro- and macroalgae are finding their way onto the food…

The classic silver mirror reaction at room temperature in textbooks usually used glucose to react with silver nitrate and ammonium nitrate with the presence of caustic alkalis. But the aldehydes such as acetaldehyde and propionaldehyde were difficult to react under the same condition. In this paper, Na[subscript 2]CO[subscript 3] was used to…

A computational experiment investigating common organic chemistry mechanisms has been developed and implemented in a junior/senior-level physical chemistry laboratory course at two institutions. Students investigated various reactions that proceed via S[subscript N]1, S[subscript N]2, E1, and E2 mechanisms using hybrid Density Functional Theory…

The Hofmeister series is a recurring trend that ranks ions' abilities to influence various aqueous processes in solution. Herein, a set of project-based experiments was developed for students in an upper-level physical chemistry laboratory to investigate the specific ion effects on the thermodynamics of caffeine partitioning between aqueous and…

The ability to visualize chemical processes can be an asset in a teaching laboratory. Despite the advances in laboratory technology, apparatuses used in the teaching of simple thermodynamics concepts, such as exothermic/endothermic reactions, historically remain unchanged and can benefit from a fresh perspective. The recent incorporation of…

We report the findings of an empirical study that investigated whether the source of data--firsthand or secondhand data gained from lab work experiments--has an influence on students' learning outcomes. Results indicate that students' choice of a correct or incorrect hypothesis for a pendulum lab experiment on the influence of the mass of the bob…

The design and operation of an inverted cone, scalable vapor condenser, drawing cooling air from beyond the boundary layer and optionally working as a part of a gastight setup, are described and discussed. Besides its main use as a reflux condenser, it can also be used in one-plate distillations.

A highly visual, inexpensive, straightforward laboratory experiment for the determination of the activation energy of a demulsification process is presented. The experiment uses low-density polyethylene (LDPE) beads to clearly mark the interface between an NaCl(aq) solution and isopropanol. The NaCl(aq)-isopropanol system is shaken to produce an…

The problem of a disc or cylinder initially rolling with slipping on a surface and subsequently transitioning to rolling without slipping is often cited in textbooks. Students struggle to qualitatively understand the difference between kinetic and static frictional forces--i.e., whereas the magnitude of the former is known, that of the latter can…

In this supplement to our second-year supercapacitor lab (Bringing Real-World Energy-Storage Research into a Second-Year Physical-Chemistry Lab Using a MnO[subscript 2]-Based Supercapacitor. "J. Chem. Educ." 2018, 95 (11), 2028-2033), we incorporate a color indicator as indirect evidence for the manganese oxide's pseudocapacitive…

A six-laboratory session biofilm-focused biochemistry laboratory module is described. Through just six four-hour laboratory sessions over three weeks, students first master background knowledge and fundamental experimental techniques to explore questions involving bacterial biofilms at the interface of microbiology and biochemistry and then…

The study of gels and their properties is a compelling topic both technologically and scientifically, and should therefore be emphasized in chemistry and material science syllabuses. In the present laboratory experiment, we propose two experiences, aimed at introducing gelation and gel transport properties using silica gels made from sodium…

A laboratory exercise on the interaction between the herbicide pendimethalin (PM) and goat serum albumin (GSA), a carrier protein present in mammalian blood circulation, is described. Fluorescence spectroscopy was used to study the binding reaction between PM and GSA. Titration of a constant amount of the protein (GSA) with increasing ligand (PM)…